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Soft Condensed Matter - Small Angle Scattering
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I22 Contact

Beamline phone numbers:
+44 (0) 1235 77 8617
+44 (0) 1235 77 8713 

Principal Beamline Scientist: 
Nick Terrill

Tel: +44 (0) 1235 778047
E-mail: [email protected]

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Science Group Leader

Robert Rambo

Email: [email protected]
Tel: +44 (0)1235 56 7675

  1. Instruments
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  3. Small Angle Scattering
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Publications

Beamline Paper

We have just published a Review of I22 Operations. It contains a description of beamline. As part of the requirement to include Diamond in your publication acknowledgements and references please include this paper for all work carried out on I22. We hope you find it useful.

User Publications

These papers are all based at least in part on data gathered on beamline I22. If you have published a paper based on data from I22 which doesn't appear here, please send a reference (ideally including a DOI) to us.

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56 items found for 2020 [total: 740]


Imaging non-classical mechanical responses of lipid membranes using molecular rotors
Miguel Paez-Perez, Ismael López-Duarte, Aurimas Vyšniauskas, Nicholas J. Brooks, Marina K. Kuimova
Chemical Science, 40 Dec 2020 DOI: 10.1039/D0SC05874B
Journal Paper I22-Small angle scattering & Diffraction open access
Microstructural, thermal, crystallization, and water absorption properties of films prepared from never‐dried and freeze‐dried cellulose nanocrystals
Kazi M. Zakir Hossain, Vincenzo Calabrese, Marcelo A. Da Silva, Julien Schmitt, Saffron J. Bryant, Md Towhidul Islam, Reda M. Felfel, Janet L. Scott, Karen Edler
Macromolecular Materials And Engineering, 10 Nov 2020 DOI: 10.1002/mame.202000462
Journal Paper I22-Small angle scattering & Diffraction open access
Fabrication and characterization of PEEK/PEI multilayer composites
Ángel Alvaredo-Atienza, Lu Chen, Verónica San-Miguel, Alvaro Ridruejo, Juan P. Fernández-Blázquez
Polymers, 12 Nov 2020 DOI: 10.3390/polym12122765
Journal Paper I22-Small angle scattering & Diffraction open access
Potassium iodide reduces the stability of triple-cation perovskite solar cells
Tarek I. Alanazi, Onkar S. Game, Joel A. Smith, Rachel C. Kilbride, Claire Greenland, Rahul Jayaprakash, Kyriacos Georgiou, Nicholas J. Terrill, David G. Lidzey
Rsc Advances, 10 Nov 2020 DOI: 10.1039/D0RA07107B
Journal Paper I22-Small angle scattering & Diffraction open access
Controlling protein nanocage assembly with hydrostatic pressure
Kristian Le Vay, Ben M. Carter, Daniel W. Watkins, T.-Y. Dora Tang, Valeska P. Ting, Helmut Cölfen, Robert P. Rambo, Andrew J. Smith, J. L. Ross Anderson, Adam W. Perriman
Journal Of The American Chemical Society, Nov 2020 DOI: 10.1021/jacs.0c07285
Journal Paper B21-High Throughput SAXS B23-Circular Dichroism I22-Small angle scattering & Diffraction
Molecular to macroscale energy absorption mechanisms in biological body armour illuminated by scanning X-ray diffraction with in situ compression
Yi Zhang, Jan Garrevoet, Yanhong Wang, Jan Torben Roeh, Nicholas J. Terrill, Gerald Falkenberg, Yuhui Dong, Himadri S. Gupta
Acs Nano, Oct 2020 DOI: 10.1021/acsnano.0c02879
Journal Paper I22-Small angle scattering & Diffraction
Solvent‐free liquid avidin as a step towards cold chain elimination
Liem Bui-Le, Alex P. S. Brogan, Jason P. Hallett
Biotechnology And Bioengineering, Oct 2020 DOI: 10.1002/bit.27587
Journal Paper B21-High Throughput SAXS B23-Circular Dichroism I22-Small angle scattering & Diffraction open access
Exploring conformational preferences of proteins: ionic liquid effects on the energy landscape of avidin
Talia A. Shmool, Laura K. Martin, Coby J. Clarke, Liem Bui-Le, Karen M. Polizzi, Jason P. Hallett
Chemical Science, 5 Oct 2020 DOI: 10.1039/D0SC04991C
Journal Paper B21-High Throughput SAXS B23-Circular Dichroism I22-Small angle scattering & Diffraction open access
Nanocrystals can cause unexpectedly violent volcanic eruptions
Diamond Light Source
Oct 2020
Science Highlight I15-Extreme Conditions I22-Small angle scattering & Diffraction
The persistence of a proxy for cooking emissions in megacities: a kinetic study of the ozonolysis of self-assembled films by simultaneous Small & Wide Angle X-ray Scattering (SAXS/WAXS) and Raman microscopy
Adam Milsom, Adam M. Squires, Ben Woden, Nicholas J. Terrill, Andrew D. Ward, Christian Pfrang
Faraday Discussions, Sept 2020 DOI: 10.1039/D0FD00088D
Journal Paper I22-Small angle scattering & Diffraction open access
In situ SAXS studies of a prototypical RAFT aqueous dispersion polymerization formulation: monitoring the evolution in copolymer morphology during polymerization-induced self-assembly
Adam Czajka, Steven P. Armes
Chemical Science, 6 Sept 2020 DOI: 10.1039/D0SC03411H
Journal Paper I22-Small angle scattering & Diffraction open access
Rational synthesis of epoxy-functional spheres, worms and vesicles by RAFT aqueous emulsion polymerisation of glycidyl methacrylate
Fiona L. Hatton, Matthew J. Derry, Steven P. Armes
Polymer Chemistry, 28 Sept 2020 DOI: 10.1039/D0PY01097A
Journal Paper I22-Small angle scattering & Diffraction open access
Structure and dynamics in ionic liquid and highly concentrated electrolytes
Filippa Lundin
Sept 2020
Thesis I22-Small angle scattering & Diffraction
A multiscale study of structural and compositional changes in a natural nanocomposite: osteoporotic bone with chronic endogenous steroid excess
Li Xi, Yi Zhang, Himadri Gupta, Nick Terrill, Pan Wang, Tian Zhao, Daining Fang
Bone, Sept 2020 DOI: 10.1016/j.bone.2020.115666
Journal Paper I22-Small angle scattering & Diffraction
In situ observation of nanolite growth in volcanic melt: A driving force for explosive eruptions
Danilo Di Genova, Richard A. Brooker, Heidy M. Mader, James W. E. Drewitt, Alessandro Longo, Joachim Deubener, Daniel R. Neuville, Sara Fanara, Olga Shebanova, Simon Anzellini, Fabio Arzilli, Emily C. Bamber, Louis Hennet, Giuseppe La Spina, Nobuyoshi Miyajima
Science Advances, 6 Sept 2020 DOI: 10.1126/sciadv.abb0413
Journal Paper I15-Extreme Conditions I22-Small angle scattering & Diffraction open access
Multiscale SAXS/WAXD characterisation of the deformation mechanisms of electrospun PCL scaffolds
F. J. Camarena-Maese, F. Martínez-Hergueta, J. P. Fernández-Blázquez, R. W. Kok, J. Reid, A. Callanan
Polymer, 203 Aug 2020 DOI: 10.1016/j.polymer.2020.122775
Journal Paper I22-Small angle scattering & Diffraction
Nanoscale mechanisms in age-related hip-fractures
Shaocheng Ma, En Lin Goh, Tabitha Tay, Crispin C. Wiles, Oliver Boughton, John H. Churchwell, Yong Wu, Angelo Karunaratne, Rajarshi Bhattacharya, Nick Terrill, Justin P. Cobb, Ulrich Hansen, Richard L. Abel
Scientific Reports, 10 Aug 2020 DOI: 10.1038/s41598-020-69783-5
Journal Paper I22-Small angle scattering & Diffraction open access
Helical networks of π‐conjugated rods – A robust design concept for bicontinuous cubic liquid crystalline phases with achiral Ia 3⎯⎯3¯d and chiral I23 lattice
Christian Dressel, Tino Reppe, Silvio Poppe, Marko Prehm, Huanjun Lu, Xiangbing Zeng, Goran Ungar, Carsten Tschierske
Advanced Functional Materials, 23 Aug 2020 DOI: 10.1002/adfm.202004353
Journal Paper I22-Small angle scattering & Diffraction open access
Self-assembled poly-catenanes from supramolecular toroidal building blocks
Sougata Datta, Yasuki Kato, Seiya Higashiharaguchi, Keisuke Aratsu, Atsushi Isobe, Takuho Saito, Deepak D. Prabhu, Yuichi Kitamoto, Martin J. Hollamby, Andrew Smith, Robert Dagleish, Najet Mahmoudi, Luca Pesce, Claudio Perego, Giovanni M. Pavan, Shiki Yagai
Nature, 583 Jul 2020 DOI: 10.1038/s41586-020-2445-z
Journal Paper I22-Small angle scattering & Diffraction
Exerting spatial control during nanoparticle occlusion within calcite crystals
Yin Ning, Yide Han, Lijuan Han, Matthew J. Derry, Steven P. Armes
Angewandte Chemie International Edition, Jul 2020 DOI: 10.1002/anie.202007110
Journal Paper I22-Small angle scattering & Diffraction
Density scaling of structure and dynamics of an ionic liquid
Henriette Wase Hansen, Filippa Lundin, Karolina Adrjanowicz, Bernhard Frick, Aleksandar Matic, Kristine Niss
Physical Chemistry Chemical Physics, 22 Jul 2020 DOI: 10.1039/D0CP01258K
Journal Paper I22-Small angle scattering & Diffraction
The influence of structure and morphology on ion permeation in commercial silicone hydrogel contact lenses
Virginia Saez‐martinez, Aisling Mann, Fiona Lydon, Frank Molock, Siân A. Layton, Daniel T. W. Toolan, Jonathan R. Howse, Paul D. Topham, Brian J. Tighe
Journal Of Biomedical Materials Research Part B: Applied Biomaterials, 18 Jul 2020 DOI: 10.1002/jbm.b.34689
Journal Paper I22-Small angle scattering & Diffraction open access
Solvent vapour annealing of methylammonium lead halide perovskite: what's the catch?
Onkar S. Game, Joel A. Smith, Tarek I. Alanazi, Michael Wong-Stringer, Vikas Kumar, Cornelia Rodenburg, Nick J. Terrill, David Lidzey
Journal Of Materials Chemistry A, 8 June 2020 DOI: 10.1039/D0TA03023F
Journal Paper I22-Small angle scattering & Diffraction
The effect of bacteriochlorophyll derivative WST-D and near infrared light on the molecular and fibrillar architecture of the corneal stroma
S. Hayes, N. Aldahlawi, A. L. Marcovich, J. Brekelmans, A. Goz, A. Scherz, R. D. Young, J. S. Bell, D. P. O’brart, R. M. M. A. Nuijts, K. M. Meek
Scientific Reports, 10 June 2020 DOI: 10.1038/s41598-020-66869-y
Journal Paper I02-Macromolecular Crystallography I22-Small angle scattering & Diffraction open access
X-ray diffraction imaging of corneal ultrastructure
Keith Meek, Andrew J. Quantock, Sally Hayes, James Bell
June 2020 DOI: 10.1007/978-1-0716-0599-8_16
Book Chapter I22-Small angle scattering & Diffraction
Synthesis of poly(stearyl methacrylate)-poly(2-hydroxypropyl methacrylate) diblock copolymer nanoparticles via RAFT dispersion polymerization of 2-hydroxypropyl methacrylate in mineral oil
Csilla György, Saul J. Hunter, Chloé Girou, Matthew Derry, Steven P. Armes
Polymer Chemistry, 68 June 2020 DOI: 10.1039/D0PY00562B
Journal Paper I22-Small angle scattering & Diffraction
The changes in bone's nanostructure associated with bone fragility & bisphosphonate treatment
Tabitha Jia Hui Tay
June 2020
Thesis I22-Small angle scattering & Diffraction open access
Enthalpic incompatibility between two steric stabilizer blocks provides control over the vesicle size distribution during polymerization-induced self-assembly in aqueous media
Deborah L. Beattie, Oleksandr O. Mykhaylyk, Steven P. Armes
Chemical Science, 45 June 2020 DOI: 10.1039/D0SC01320J
Journal Paper I22-Small angle scattering & Diffraction open access
Ensilicated tetanus antigen retains immunogenicity: in vivo study and time-resolved SAXS characterization
A. Doekhie, R. Dattani, Y-C. Chen, Y. Yang, A. Smith, A. P. Silve, F. Koumanov, S. A. Wells, K. J. Edler, K. J. Marchbank, J. M. H. Van Den Elsen, A. Sartbaeva
Scientific Reports, 10 June 2020 DOI: 10.1038/s41598-020-65876-3
Journal Paper I22-Small angle scattering & Diffraction open access
Mechanical response of cortical bone in compression and tension at the mineralized fibrillar level in steroid induced osteoporosis
Li Xi, Weibin Wen, Wenwang Wu, Zhaoliang Qu, Ran Tao, Angelo Karunaratne, Binbin Liao, Ying Liu, Daining Fang
Composites Part B: Engineering, May 2020 DOI: 10.1016/j.compositesb.2020.108138
Journal Paper I22-Small angle scattering & Diffraction
Triblock polyester thermoplastic elastomers with semi-aromatic polymer end blocks by ring-opening copolymerization
Georgina L. Gregory, Gregory S. Sulley, Leticia Peña Carrodeguas, Thomas T. D. Chen, Alba Santmarti, Nicholas J. Terrill, Koon-Yang Lee, Charlotte K. Williams
Chemical Science, 50 May 2020 DOI: 10.1039/D0SC00463D
Journal Paper I22-Small angle scattering & Diffraction open access
Aromatic stacking facilitated self-assembly of ultra-short ionic complementary peptide sequence: β-sheet nanofibres with remarkable gelation and interfacial properties
Jacek K. Wychowaniec, Ronak Patel, James Leach, Rachel Mathomes, Vikesh Chhabria, Yogita Patil-Sen, Araida Hidalgo-Bastida, Robert T. Forbes, Joseph M. Hayes, Mohamed A. Elsawy
Biomacromolecules, May 2020 DOI: 10.1021/acs.biomac.0c00366
Journal Paper I22-Small angle scattering & Diffraction open access
Tailoring liquid crystal honeycombs by head-group choice in bird-like bent-core mesogens
Ya-Xin Li, Huifang Cheng, Xiangbing Zeng, Yuan Tao, Xiaohong Cheng, Goran Ungar
Journal Of Materials Chemistry C, 106 May 2020 DOI: 10.1039/D0TC01879A
Journal Paper I16-Materials and Magnetism I22-Small angle scattering & Diffraction open access
A facile method for generating worm-like micelles with controlled lengths and narrow polydispersity
Ouassef Nahi, Olivier J. Cayre, Yi-Yeoun Kim, Andrew J. Smith, Nicholas J. Warren, Fiona C. Meldrum
Chemical Communications, 44 May 2020 DOI: 10.1039/D0CC02313B
Journal Paper I22-Small angle scattering & Diffraction open access
Biophysical differences between COPD, CF and healthy airways mucus
Vladislav Genevskiy
May 2020
Thesis I22-Small angle scattering & Diffraction
Using state-of-the-art nanocarriers to beat bacterial resistance
Diamond Light Source
May 2020
Science Highlight I22-Small angle scattering & Diffraction
In-situ uniaxial drawing of poly-L-lactic acid (PLLA): Following the crystalline morphology development using time-resolved SAXS/WAXS
Ellen L. Heeley, Kharmen Billimoria, Nathan Parsons, Lukasz Figiel, Elspeth M. Keating, Conor T. Cafolla, Eleanor M. Crabb, Darren J. Hughes
Polymer, 193 Apr 2020 DOI: 10.1016/j.polymer.2020.122353
Journal Paper I22-Small angle scattering & Diffraction
Ionic and nonspherical polymer nanoparticles in nonpolar solvents
Gregory N. Smith, Sarah L. Canning, Matthew J. Derry, Elizabeth R. Jones, Thomas J. Neal, Andrew J. Smith
Macromolecules, Apr 2020 DOI: 10.1021/acs.macromol.0c00121
Journal Paper I22-Small angle scattering & Diffraction
Inter-α-inhibitor heavy chain-1 has an integrin-like 3D structure mediating immune regulatory activities and matrix stabilization during ovulation
Jan J. Enghild, Clair Baldock, Caroline M. Milner, Anthony J. Day, David C. Briggs, Alexander W. W. Langford-Smith, Holly L. Birchenough, Thomas A. Jowitt, Cay M. Kielty
Journal Of Biological Chemistry, Apr 2020 DOI: 10.1074/jbc.RA119.011916
Journal Paper I03-Macromolecular Crystallography I22-Small angle scattering & Diffraction open access
Influence of an ionic comonomer on polymerization-induced self-assembly of diblock copolymers in non-polar media
Gregory N. Smith, Sarah L. Canning, Matthew J. Derry, Oleksandr O. Mykhaylyk, Sarah E. Norman, Steven P. Armes
Polymer Chemistry, 11 Apr 2020 DOI: 10.1039/D0PY00101E
Journal Paper I22-Small angle scattering & Diffraction
Role of sheet-edge interactions in β-sheet self-assembling peptide hydrogels
Jacek K. Wychowaniec, Andrew Smith, Cosimo Ligorio, Oleksandr O. Mykhaylyk, Aline F. Miller, Alberto Saiani
Biomacromolecules, Apr 2020 DOI: 10.1021/acs.biomac.0c00229
Journal Paper I22-Small angle scattering & Diffraction open access
Nucleation pathway of calcium sulfate hemihydrate (bassanite) from solution: Implications for calcium sulfates on Mars
Tomasz M. Stawski, Rogier Besselink, Konstantinos Chatzipanagis, Jorn Hovelmann, Liane G. Benning, Alexander E. S. Van Driessche
The Journal Of Physical Chemistry C, Mar 2020 DOI: 10.1021/acs.jpcc.0c01041
Journal Paper I22-Small angle scattering & Diffraction
Developmental abnormalities in the cornea of a mouse model for Marfan syndrome
Eleanor Feneck, Rodrigo B. Souza, Philip N. Lewis, Sally Hayes, Lygia V. Pereira, Keith M. Meek
Experimental Eye Research, Mar 2020 DOI: 10.1016/j.exer.2020.108001
Journal Paper I22-Small angle scattering & Diffraction open access
Investigation of bone matrix composition, architecture and mechanical properties reflect structure-function relationship of cortical bone in glucocorticoid induced osteoporosis
Li Xi, Yu Song, Wenwang Wu, Zhaoliang Qu, Jiawei Wen, Binbin Liao, Ran Tao, Jingran Ge, Daining Fang
Bone, Mar 2020 DOI: 10.1016/j.bone.2020.115334
Journal Paper I22-Small angle scattering & Diffraction
Double‐gyroid nanostructure formation by aggregation‐induced atropisomerization and co‐assembly of ionic liquid‐crystalline amphiphiles
Nanami Uemura, Tsubasa Kobayashi, Shintaro Yoshida, Ya‐xin Li, Karel Goossens, Xiangbing Zeng, Go Watanabe, Takahiro Ichikawa
Angewandte Chemie International Edition, 1 Mar 2020 DOI: 10.1002/anie.202000424
Journal Paper I22-Small angle scattering & Diffraction open access
Switchable catalysis improves the properties of co 2 -derived polymers: Poly(cyclohexene carbonate- b -ε-decalactone- b -cyclohexene carbonate) adhesives, elastomers, and toughened plastics
Gregory S. Sulley, Georgina L. Gregory, Thomas T. D. Chen, Leticia Peña Carrodeguas, Gemma Trott, Alba Santmarti, Koon-Yang Lee, Nicholas J. Terrill, Charlotte K. Williams
Journal Of The American Chemical Society, Feb 2020 DOI: 10.1021/jacs.9b13106
Journal Paper I22-Small angle scattering & Diffraction open access
RAFT dispersion polymerization of benzyl methacrylate in silicone oil using a silicone-based methacrylic stabilizer provides convenient access to spheres, worms, and vesicles
Matthew J. Rymaruk, Cate T. O'Brien, Steven L. Brown, Clive N. Williams, Steven P. Armes
Macromolecules, Feb 2020 DOI: 10.1021/acs.macromol.9b02697
Journal Paper I22-Small angle scattering & Diffraction
Core-shell spheroidal hydrogels produced via charge-driven interfacial complexation
Vincenzo Calabrese, Davide Califano, Marcelo A. Da Silva, Julien Schmitt, Saffron J. Bryant, Kazi M. Zakir Hossain, Ana Maria Percebom, Aurora Perez-Gramatges, Janet Lesley Scott, Karen J. Edler
Acs Applied Polymer Materials, Feb 2020 DOI: 10.1021/acsapm.9b01086
Journal Paper I22-Small angle scattering & Diffraction open access
Liquid organic frameworks: The single-network “plumber’s nightmare” bicontinuous cubic liquid crystal
Silvio Poppe, Xiaohong Cheng, Changlong Chen, Xiangbing Zeng, Rui-Bin Zhang, Feng Liu, Goran Ungar, Carsten Tschierske
Journal Of The American Chemical Society, Feb 2020 DOI: 10.1021/jacs.9b11073
Journal Paper I22-Small angle scattering & Diffraction
Hydrophobization of cellulose nanocrystals for aqueous colloidal suspensions and gels
Rinat Nigmatullin, Marcus A. Johns, Juan C. Muñoz-García, Valeria Gabrielli, Julien Schmitt, Jesús Angulo, Yaroslav Z. Khimyak, Janet Lesley Scott, Karen J. Edler, Stephen J. Eichhorn
Biomacromolecules, Jan 2020 DOI: 10.1021/acs.biomac.9b01721
Journal Paper I22-Small angle scattering & Diffraction
Structural changes in lipid mesophases due to intercalation of dendritic polymer nanoparticles: Swollen lamellae, suppressed curvature, and augmented structural disorder
Laura J. Fox, Lauren Matthews, Holly Stockdale, Supakit Pichai, Tim Snow, Robert M. Richardson, Wuge H. Briscoe
Acta Biomaterialia, Jan 2020 DOI: 10.1016/j.actbio.2019.12.036
Journal Paper I22-Small angle scattering & Diffraction
RAFT dispersion polymerisation of lauryl methacrylate in ethanol–water binary mixtures: synthesis of diblock copolymer vesicles with deformable membranes
R. R. Gibson, E. J. Cornel, O. M. Musa, A. Fernyhough, S. P. Armes
Polymer Chemistry, 54 Jan 2020 DOI: 10.1039/C9PY01768B
Journal Paper I22-Small angle scattering & Diffraction
Making simulated cosmic dust - in the microwave!
Diamond Light Source
Jan 2020
Science Highlight I11-High Resolution Powder Diffraction I22-Small angle scattering & Diffraction
Three-dimensional studies of the developing mammalian cornea
Eleanor Feneck
Jan 2020
Thesis I22-Small angle scattering & Diffraction
Structural changes in the eye lens during accommodation
Saleha Al-Atawi
Jan 2020
Thesis I22-Small angle scattering & Diffraction
Synchrotron X-ray nanomechanical imaging applied to multiscale deformation in biological armour
Yanhong Wang
Jan 2020
Thesis I22-Small angle scattering & Diffraction
  1. Miguel Paez-Perez, Ismael López-Duarte, Aurimas Vyšniauskas, Nicholas J. Brooks, Marina K. Kuimova, "Imaging non-classical mechanical responses of lipid membranes using molecular rotors", Chemical Science, 40 (2020), DOI: 10.1039/D0SC05874B
  2. Kazi M. Zakir Hossain, Vincenzo Calabrese, Marcelo A. Da Silva, Julien Schmitt, Saffron J. Bryant, Md Towhidul Islam, Reda M. Felfel, Janet L. Scott, Karen Edler, "Microstructural, thermal, crystallization, and water absorption properties of films prepared from never‐dried and freeze‐dried cellulose nanocrystals", Macromolecular Materials And Engineering, 10 (2020), DOI: 10.1002/mame.202000462
  3. Ángel Alvaredo-Atienza, Lu Chen, Verónica San-Miguel, Alvaro Ridruejo, Juan P. Fernández-Blázquez, "Fabrication and characterization of PEEK/PEI multilayer composites", Polymers, 12 (2020), DOI: 10.3390/polym12122765
  4. Tarek I. Alanazi, Onkar S. Game, Joel A. Smith, Rachel C. Kilbride, Claire Greenland, Rahul Jayaprakash, Kyriacos Georgiou, Nicholas J. Terrill, David G. Lidzey, "Potassium iodide reduces the stability of triple-cation perovskite solar cells", Rsc Advances, 10, 40341 - 40350 (2020), DOI: 10.1039/D0RA07107B
  5. Kristian Le Vay, Ben M. Carter, Daniel W. Watkins, T.-Y. Dora Tang, Valeska P. Ting, Helmut Cölfen, Robert P. Rambo, Andrew J. Smith, J. L. Ross Anderson, Adam W. Perriman, "Controlling protein nanocage assembly with hydrostatic pressure", Journal Of The American Chemical Society (2020), DOI: 10.1021/jacs.0c07285
  6. Yi Zhang, Jan Garrevoet, Yanhong Wang, Jan Torben Roeh, Nicholas J. Terrill, Gerald Falkenberg, Yuhui Dong, Himadri S. Gupta, "Molecular to macroscale energy absorption mechanisms in biological body armour illuminated by scanning X-ray diffraction with in situ compression", Acs Nano (2020), DOI: 10.1021/acsnano.0c02879
  7. Liem Bui-Le, Alex P. S. Brogan, Jason P. Hallett, "Solvent‐free liquid avidin as a step towards cold chain elimination", Biotechnology And Bioengineering (2020), DOI: 10.1002/bit.27587
  8. Talia A. Shmool, Laura K. Martin, Coby J. Clarke, Liem Bui-Le, Karen M. Polizzi, Jason P. Hallett, "Exploring conformational preferences of proteins: ionic liquid effects on the energy landscape of avidin", Chemical Science, 5 (2020), DOI: 10.1039/D0SC04991C
  9. [Science Highlight] Diamond Light Source, "Nanocrystals can cause unexpectedly violent volcanic eruptions" (2020)
  10. Adam Milsom, Adam M. Squires, Ben Woden, Nicholas J. Terrill, Andrew D. Ward, Christian Pfrang, "The persistence of a proxy for cooking emissions in megacities: a kinetic study of the ozonolysis of self-assembled films by simultaneous Small & Wide Angle X-ray Scattering (SAXS/WAXS) and Raman microscopy", Faraday Discussions (2020), DOI: 10.1039/D0FD00088D
  11. Adam Czajka, Steven P. Armes, "In situ SAXS studies of a prototypical RAFT aqueous dispersion polymerization formulation: monitoring the evolution in copolymer morphology during polymerization-induced self-assembly", Chemical Science, 6 (2020), DOI: 10.1039/D0SC03411H
  12. Fiona L. Hatton, Matthew J. Derry, Steven P. Armes, "Rational synthesis of epoxy-functional spheres, worms and vesicles by RAFT aqueous emulsion polymerisation of glycidyl methacrylate", Polymer Chemistry, 28 (2020), DOI: 10.1039/D0PY01097A
  13. [Thesis] Filippa Lundin, "Structure and dynamics in ionic liquid and highly concentrated electrolytes" (2020)
  14. Li Xi, Yi Zhang, Himadri Gupta, Nick Terrill, Pan Wang, Tian Zhao, Daining Fang, "A multiscale study of structural and compositional changes in a natural nanocomposite: osteoporotic bone with chronic endogenous steroid excess", Bone (2020), DOI: 10.1016/j.bone.2020.115666
  15. Danilo Di Genova, Richard A. Brooker, Heidy M. Mader, James W. E. Drewitt, Alessandro Longo, Joachim Deubener, Daniel R. Neuville, Sara Fanara, Olga Shebanova, Simon Anzellini, Fabio Arzilli, Emily C. Bamber, Louis Hennet, Giuseppe La Spina, Nobuyoshi Miyajima, "In situ observation of nanolite growth in volcanic melt: A driving force for explosive eruptions", Science Advances, 6 (2020), DOI: 10.1126/sciadv.abb0413
  16. F. J. Camarena-Maese, F. Martínez-Hergueta, J. P. Fernández-Blázquez, R. W. Kok, J. Reid, A. Callanan, "Multiscale SAXS/WAXD characterisation of the deformation mechanisms of electrospun PCL scaffolds", Polymer, 203 (2020), DOI: 10.1016/j.polymer.2020.122775
  17. Shaocheng Ma, En Lin Goh, Tabitha Tay, Crispin C. Wiles, Oliver Boughton, John H. Churchwell, Yong Wu, Angelo Karunaratne, Rajarshi Bhattacharya, Nick Terrill, Justin P. Cobb, Ulrich Hansen, Richard L. Abel, "Nanoscale mechanisms in age-related hip-fractures", Scientific Reports, 10 (2020), DOI: 10.1038/s41598-020-69783-5
  18. Christian Dressel, Tino Reppe, Silvio Poppe, Marko Prehm, Huanjun Lu, Xiangbing Zeng, Goran Ungar, Carsten Tschierske, "Helical networks of π‐conjugated rods – A robust design concept for bicontinuous cubic liquid crystalline phases with achiral Ia 3⎯⎯3¯d and chiral I23 lattice", Advanced Functional Materials, 23 (2020), DOI: 10.1002/adfm.202004353
  19. Sougata Datta, Yasuki Kato, Seiya Higashiharaguchi, Keisuke Aratsu, Atsushi Isobe, Takuho Saito, Deepak D. Prabhu, Yuichi Kitamoto, Martin J. Hollamby, Andrew Smith, Robert Dagleish, Najet Mahmoudi, Luca Pesce, Claudio Perego, Giovanni M. Pavan, Shiki Yagai, "Self-assembled poly-catenanes from supramolecular toroidal building blocks", Nature, 583, 400 - 405 (2020), DOI: 10.1038/s41586-020-2445-z
  20. Yin Ning, Yide Han, Lijuan Han, Matthew J. Derry, Steven P. Armes, "Exerting spatial control during nanoparticle occlusion within calcite crystals", Angewandte Chemie International Edition (2020), DOI: 10.1002/anie.202007110
  21. Henriette Wase Hansen, Filippa Lundin, Karolina Adrjanowicz, Bernhard Frick, Aleksandar Matic, Kristine Niss, "Density scaling of structure and dynamics of an ionic liquid", Physical Chemistry Chemical Physics, 22, 14169 - 14176 (2020), DOI: 10.1039/D0CP01258K
  22. Virginia Saez‐martinez, Aisling Mann, Fiona Lydon, Frank Molock, Siân A. Layton, Daniel T. W. Toolan, Jonathan R. Howse, Paul D. Topham, Brian J. Tighe, "The influence of structure and morphology on ion permeation in commercial silicone hydrogel contact lenses", Journal Of Biomedical Materials Research Part B: Applied Biomaterials, 18 (2020), DOI: 10.1002/jbm.b.34689
  23. Onkar S. Game, Joel A. Smith, Tarek I. Alanazi, Michael Wong-Stringer, Vikas Kumar, Cornelia Rodenburg, Nick J. Terrill, David Lidzey, "Solvent vapour annealing of methylammonium lead halide perovskite: what's the catch?", Journal Of Materials Chemistry A, 8, 10943 - 10956 (2020), DOI: 10.1039/D0TA03023F
  24. S. Hayes, N. Aldahlawi, A. L. Marcovich, J. Brekelmans, A. Goz, A. Scherz, R. D. Young, J. S. Bell, D. P. O’brart, R. M. M. A. Nuijts, K. M. Meek, "The effect of bacteriochlorophyll derivative WST-D and near infrared light on the molecular and fibrillar architecture of the corneal stroma", Scientific Reports, 10 (2020), DOI: 10.1038/s41598-020-66869-y
  25. [Book Chapter] Keith Meek, Andrew J. Quantock, Sally Hayes, James Bell, "X-ray diffraction imaging of corneal ultrastructure" (2020), DOI: 10.1007/978-1-0716-0599-8_16
  26. Csilla György, Saul J. Hunter, Chloé Girou, Matthew Derry, Steven P. Armes, "Synthesis of poly(stearyl methacrylate)-poly(2-hydroxypropyl methacrylate) diblock copolymer nanoparticles via RAFT dispersion polymerization of 2-hydroxypropyl methacrylate in mineral oil", Polymer Chemistry, 68 (2020), DOI: 10.1039/D0PY00562B
  27. [Thesis] Tabitha Jia Hui Tay, "The changes in bone's nanostructure associated with bone fragility & bisphosphonate treatment" (2020)
  28. Deborah L. Beattie, Oleksandr O. Mykhaylyk, Steven P. Armes, "Enthalpic incompatibility between two steric stabilizer blocks provides control over the vesicle size distribution during polymerization-induced self-assembly in aqueous media", Chemical Science, 45 (2020), DOI: 10.1039/D0SC01320J
  29. A. Doekhie, R. Dattani, Y-C. Chen, Y. Yang, A. Smith, A. P. Silve, F. Koumanov, S. A. Wells, K. J. Edler, K. J. Marchbank, J. M. H. Van Den Elsen, A. Sartbaeva, "Ensilicated tetanus antigen retains immunogenicity: in vivo study and time-resolved SAXS characterization", Scientific Reports, 10 (2020), DOI: 10.1038/s41598-020-65876-3
  30. Li Xi, Weibin Wen, Wenwang Wu, Zhaoliang Qu, Ran Tao, Angelo Karunaratne, Binbin Liao, Ying Liu, Daining Fang, "Mechanical response of cortical bone in compression and tension at the mineralized fibrillar level in steroid induced osteoporosis", Composites Part B: Engineering (2020), DOI: 10.1016/j.compositesb.2020.108138
  31. Georgina L. Gregory, Gregory S. Sulley, Leticia Peña Carrodeguas, Thomas T. D. Chen, Alba Santmarti, Nicholas J. Terrill, Koon-Yang Lee, Charlotte K. Williams, "Triblock polyester thermoplastic elastomers with semi-aromatic polymer end blocks by ring-opening copolymerization", Chemical Science, 50 (2020), DOI: 10.1039/D0SC00463D
  32. Jacek K. Wychowaniec, Ronak Patel, James Leach, Rachel Mathomes, Vikesh Chhabria, Yogita Patil-Sen, Araida Hidalgo-Bastida, Robert T. Forbes, Joseph M. Hayes, Mohamed A. Elsawy, "Aromatic stacking facilitated self-assembly of ultra-short ionic complementary peptide sequence: β-sheet nanofibres with remarkable gelation and interfacial properties", Biomacromolecules (2020), DOI: 10.1021/acs.biomac.0c00366
  33. Ya-Xin Li, Huifang Cheng, Xiangbing Zeng, Yuan Tao, Xiaohong Cheng, Goran Ungar, "Tailoring liquid crystal honeycombs by head-group choice in bird-like bent-core mesogens", Journal Of Materials Chemistry C, 106 (2020), DOI: 10.1039/D0TC01879A
  34. Ouassef Nahi, Olivier J. Cayre, Yi-Yeoun Kim, Andrew J. Smith, Nicholas J. Warren, Fiona C. Meldrum, "A facile method for generating worm-like micelles with controlled lengths and narrow polydispersity", Chemical Communications, 44 (2020), DOI: 10.1039/D0CC02313B
  35. [Thesis] Vladislav Genevskiy, "Biophysical differences between COPD, CF and healthy airways mucus" (2020)
  36. [Science Highlight] Diamond Light Source, "Using state-of-the-art nanocarriers to beat bacterial resistance" (2020)
  37. Ellen L. Heeley, Kharmen Billimoria, Nathan Parsons, Lukasz Figiel, Elspeth M. Keating, Conor T. Cafolla, Eleanor M. Crabb, Darren J. Hughes, "In-situ uniaxial drawing of poly-L-lactic acid (PLLA): Following the crystalline morphology development using time-resolved SAXS/WAXS", Polymer, 193 (2020), DOI: 10.1016/j.polymer.2020.122353
  38. Gregory N. Smith, Sarah L. Canning, Matthew J. Derry, Elizabeth R. Jones, Thomas J. Neal, Andrew J. Smith, "Ionic and nonspherical polymer nanoparticles in nonpolar solvents", Macromolecules (2020), DOI: 10.1021/acs.macromol.0c00121
  39. Jan J. Enghild, Clair Baldock, Caroline M. Milner, Anthony J. Day, David C. Briggs, Alexander W. W. Langford-Smith, Holly L. Birchenough, Thomas A. Jowitt, Cay M. Kielty, "Inter-α-inhibitor heavy chain-1 has an integrin-like 3D structure mediating immune regulatory activities and matrix stabilization during ovulation", Journal Of Biological Chemistry (2020), DOI: 10.1074/jbc.RA119.011916
  40. Gregory N. Smith, Sarah L. Canning, Matthew J. Derry, Oleksandr O. Mykhaylyk, Sarah E. Norman, Steven P. Armes, "Influence of an ionic comonomer on polymerization-induced self-assembly of diblock copolymers in non-polar media", Polymer Chemistry, 11, 2605 - 2614 (2020), DOI: 10.1039/D0PY00101E
  41. Jacek K. Wychowaniec, Andrew Smith, Cosimo Ligorio, Oleksandr O. Mykhaylyk, Aline F. Miller, Alberto Saiani, "Role of sheet-edge interactions in β-sheet self-assembling peptide hydrogels", Biomacromolecules (2020), DOI: 10.1021/acs.biomac.0c00229
  42. Tomasz M. Stawski, Rogier Besselink, Konstantinos Chatzipanagis, Jorn Hovelmann, Liane G. Benning, Alexander E. S. Van Driessche, "Nucleation pathway of calcium sulfate hemihydrate (bassanite) from solution: Implications for calcium sulfates on Mars", The Journal Of Physical Chemistry C (2020), DOI: 10.1021/acs.jpcc.0c01041
  43. Eleanor Feneck, Rodrigo B. Souza, Philip N. Lewis, Sally Hayes, Lygia V. Pereira, Keith M. Meek, "Developmental abnormalities in the cornea of a mouse model for Marfan syndrome", Experimental Eye Research (2020), DOI: 10.1016/j.exer.2020.108001
  44. Li Xi, Yu Song, Wenwang Wu, Zhaoliang Qu, Jiawei Wen, Binbin Liao, Ran Tao, Jingran Ge, Daining Fang, "Investigation of bone matrix composition, architecture and mechanical properties reflect structure-function relationship of cortical bone in glucocorticoid induced osteoporosis", Bone (2020), DOI: 10.1016/j.bone.2020.115334
  45. Nanami Uemura, Tsubasa Kobayashi, Shintaro Yoshida, Ya‐xin Li, Karel Goossens, Xiangbing Zeng, Go Watanabe, Takahiro Ichikawa, "Double‐gyroid nanostructure formation by aggregation‐induced atropisomerization and co‐assembly of ionic liquid‐crystalline amphiphiles", Angewandte Chemie International Edition, 1 (2020), DOI: 10.1002/anie.202000424
  46. Gregory S. Sulley, Georgina L. Gregory, Thomas T. D. Chen, Leticia Peña Carrodeguas, Gemma Trott, Alba Santmarti, Koon-Yang Lee, Nicholas J. Terrill, Charlotte K. Williams, "Switchable catalysis improves the properties of co 2 -derived polymers: Poly(cyclohexene carbonate- b -ε-decalactone- b -cyclohexene carbonate) adhesives, elastomers, and toughened plastics", Journal Of The American Chemical Society (2020), DOI: 10.1021/jacs.9b13106
  47. Matthew J. Rymaruk, Cate T. O'Brien, Steven L. Brown, Clive N. Williams, Steven P. Armes, "RAFT dispersion polymerization of benzyl methacrylate in silicone oil using a silicone-based methacrylic stabilizer provides convenient access to spheres, worms, and vesicles", Macromolecules (2020), DOI: 10.1021/acs.macromol.9b02697
  48. Vincenzo Calabrese, Davide Califano, Marcelo A. Da Silva, Julien Schmitt, Saffron J. Bryant, Kazi M. Zakir Hossain, Ana Maria Percebom, Aurora Perez-Gramatges, Janet Lesley Scott, Karen J. Edler, "Core-shell spheroidal hydrogels produced via charge-driven interfacial complexation", Acs Applied Polymer Materials (2020), DOI: 10.1021/acsapm.9b01086
  49. Silvio Poppe, Xiaohong Cheng, Changlong Chen, Xiangbing Zeng, Rui-Bin Zhang, Feng Liu, Goran Ungar, Carsten Tschierske, "Liquid organic frameworks: The single-network “plumber’s nightmare” bicontinuous cubic liquid crystal", Journal Of The American Chemical Society (2020), DOI: 10.1021/jacs.9b11073
  50. Rinat Nigmatullin, Marcus A. Johns, Juan C. Muñoz-García, Valeria Gabrielli, Julien Schmitt, Jesús Angulo, Yaroslav Z. Khimyak, Janet Lesley Scott, Karen J. Edler, Stephen J. Eichhorn, "Hydrophobization of cellulose nanocrystals for aqueous colloidal suspensions and gels", Biomacromolecules (2020), DOI: 10.1021/acs.biomac.9b01721
  51. Laura J. Fox, Lauren Matthews, Holly Stockdale, Supakit Pichai, Tim Snow, Robert M. Richardson, Wuge H. Briscoe, "Structural changes in lipid mesophases due to intercalation of dendritic polymer nanoparticles: Swollen lamellae, suppressed curvature, and augmented structural disorder", Acta Biomaterialia (2020), DOI: 10.1016/j.actbio.2019.12.036
  52. R. R. Gibson, E. J. Cornel, O. M. Musa, A. Fernyhough, S. P. Armes, "RAFT dispersion polymerisation of lauryl methacrylate in ethanol–water binary mixtures: synthesis of diblock copolymer vesicles with deformable membranes", Polymer Chemistry, 54 (2020), DOI: 10.1039/C9PY01768B
  53. [Science Highlight] Diamond Light Source, "Making simulated cosmic dust - in the microwave!" (2020)
  54. [Thesis] Eleanor Feneck, "Three-dimensional studies of the developing mammalian cornea" (2020)
  55. [Thesis] Saleha Al-Atawi, "Structural changes in the eye lens during accommodation" (2020)
  56. [Thesis] Yanhong Wang, "Synchrotron X-ray nanomechanical imaging applied to multiscale deformation in biological armour" (2020)

Beamline Technical Publications

SAXS Roadmap for Diamond (June 2004) (420 KB)

Beamline 11: A non-crystalline diffraction beamline for the physical and life sciences on Diamond (July 2001) (269 KB)

Detailed Proposal for the Non Crystalline Diffraction Beamline (July 2001) (760 KB)

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Diamond Light Source is the UK's national synchrotron science facility, located at the Harwell Science and Innovation Campus in Oxfordshire.

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Harwell Science & Innovation Campus
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OX11 0DE

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