Instruments by Science Group
Macromolecular
Soft Condensed 
Imaging and
Biological
Magnetic
Structures and
Crystallography 
Spectroscopy I22 Contact
Beamline phone numbers:
+44 (0) 1235 77 8617
+44 (0) 1235 77 8713
Principal Beamline Scientist:
Nick Terrill
Tel: +44 (0) 1235 778047
E-mail: [email protected]
Science Group Leader
Robert Rambo
Email: [email protected]
Tel: +44 (0)1235 56 7675
Beamline Paper
We have just published a Review of I22 Operations. It contains a description of beamline. As part of the requirement to include Diamond in your publication acknowledgements and references please include this paper for all work carried out on I22. We hope you find it useful.
User Publications
These papers are all based at least in part on data gathered on beamline I22. If you have published a paper based on data from I22 which doesn't appear here, please send a reference (ideally including a DOI) to us.
49 items found for 2016 [total: 740]
Not just fractal surfaces, but surface fractal aggregates: Derivation of the expression for the structure factor and its applications The Journal Of Chemical Physics, 145 Dec 2016 DOI: 10.1063/1.4960953
The Streptococcus gordonii adhesin CshA binds host fibronectin via a catch-clamp mechanism Journal Of Biological Chemistry, Dec 2016 DOI: 10.1074/jbc.M116.760975
Journal Paper I03-Macromolecular Crystallography I04-1-Macromolecular Crystallography (fixed wavelength) I22-Small angle scattering & Diffraction open access
Overexpression of TIMP-3 in chondrocytes produces transient reduction in growth plate length but permanently reduces adult bone quality and quantity Plos One, 11 Dec 2016 DOI: 10.1371/journal.pone.0167971
Liquid crystalline phases in suspensions of pigments in non-polar solvents Dec 2016 DOI: 10.1142/9789814619264_0026
Book Chapter I22-Small angle scattering & Diffraction
Structural studies of the corneal stroma with focus on the elastic fibre network in health and disease Nov 2016
Thesis I02-Macromolecular Crystallography I22-Small angle scattering & Diffraction open access
ABC triblock copolymer worms: synthesis, characterization, and evaluation as pickering emulsifiers for millimeter-sized droplets Macromolecules, 49 Oct 2016 DOI: 10.1021/acs.macromol.6b01729
Interfibrillar stiffening of echinoderm mutable collagenous tissue demonstrated at the nanoscale Proceedings Of The National Academy Of Sciences, Oct 2016 DOI: 10.1073/pnas.1609341113
The internal structure of poly(methyl methacrylate) latexes in nonpolar solvents Journal Of Colloid And Interface Science, 479 Oct 2016 DOI: 10.1016/j.jcis.2016.06.027
Journal Paper I22-Small angle scattering & Diffraction
Superflexibility of graphene oxide Proceedings Of The National Academy Of Sciences, 113 Sept 2016 DOI: 10.1073/pnas.1605121113
Journal Paper I22-Small angle scattering & Diffraction
Body-centred cubic packing of spheres – the ultimate thermotropic assembly mode for highly divergent dendrons Nanoscale Horizons, 2 Sept 2016 DOI: 10.1039/C6NH00155F
Multiscale structure and mechanics of bone in glucocorticoid induced osteoporosis Sept 2016
Thesis I22-Small angle scattering & Diffraction
Self-assembly and template-directed synthesis in multi-strand porphyrin arrays Sept 2016
Thesis I22-Small angle scattering & Diffraction open access
Neurofilaments function as shock absorbers: compression response arising from disordered proteins Physical Review Letters, 117 Sept 2016 DOI: 10.1103/PhysRevLett.117.148101
Journal Paper I22-Small angle scattering & Diffraction
Structural transition in myelin membrane as initiator of multiple sclerosis Journal Of The American Chemical Society, 138 Sept 2016 DOI: 10.1021/jacs.6b04826
Journal Paper I22-Small angle scattering & Diffraction
Hard and soft nanomaterial films Sept 2016
Thesis I07-Surface & interface diffraction I22-Small angle scattering & Diffraction
Polymerisation-induced self-assembly in non-polar solvents Sept 2016
Thesis I22-Small angle scattering & Diffraction
Mechanisms of polymer-templated nanoparticle synthesis: contrasting ZnS and Au Langmuir, Aug 2016 DOI: 10.1021/acs.langmuir.6b01900
Ferrihydrite formation: the role of Fe13 Keggin clusters Environmental Science & Technology, Aug 2016 DOI: 10.1021/acs.est.6b02481
Probing multi-scale mechanical damage in connective tissues using x-ray diffraction Acta Biomaterialia, Aug 2016 DOI: 10.1016/j.actbio.2016.08.027
Tuning the interaction of nanoparticles from repulsive to attractive by pressure The Journal Of Physical Chemistry C, Aug 2016 DOI: 10.1021/acs.jpcc.6b06847
Journal Paper I22-Small angle scattering & Diffraction
Making gold metamaterials with a twist Aug 2016
Diamond Annual Review Highlight B23-Circular Dichroism I16-Materials and Magnetism I22-Small angle scattering & Diffraction
Hybrid glasses: A new family of glasses captured with small angle X-ray scattering and calorimetry Aug 2016
Diamond Annual Review Highlight I15-Extreme Conditions I22-Small angle scattering & Diffraction
Determining the effective density and stabilizer layer thickness of sterically stabilized nanoparticles Macromolecules, Jul 2016 DOI: 10.1021/acs.macromol.6b00987
Simultaneous SAXS and SANS analysis for the detection of toroidal supramolecular polymers composed of noncovalent supermacrocycles in solution Angewandte Chemie International Edition, Jul 2016 DOI: 10.1002/anie.201603370
Journal Paper I22-Small angle scattering & Diffraction
Ligand layer engineering to control stability and interfacial properties of nanoparticles Langmuir, Jul 2016 DOI: 10.1021/acs.langmuir.6b01704
Journal Paper I22-Small angle scattering & Diffraction
Understanding gypsum growth Jul 2016
Science Highlight I22-Small angle scattering & Diffraction
Hydrophilic nanoparticles stabilising mesophase curvature at low concentration but disrupting mesophase order at higher concentrations Soft Matter, June 2016 DOI: 10.1039/C6SM00393A
Formation of a double diamond cubic phase by thermotropic liquid crystalline self-assembly of bundled bolaamphiphiles Angewandte Chemie International Edition, June 2016 DOI: 10.1002/anie.201602734
Microfluidic SAXS study of lamellar and multilamellar vesicle phases of linear sodium alkylbenzenesulfonate surfactant with intrinsic isomeric distribution Langmuir, 32 (23) June 2016 DOI: 10.1021/acs.langmuir.6b01240
An investigation into the hexagonal phases formed in high-concentration dispersions of well-defined cylindrical block copolymer micelles Liquid Crystals, May 2016 DOI: 10.1080/02678292.2016.1170217
Journal Paper I22-Small angle scattering & Diffraction
Uncovering three-dimensional gradients in fibrillar orientation in an impact-resistant biological armour Scientific Reports, 6 May 2016 DOI: 10.1038/srep26249
Monitoring the formation of a CH3NH3PbI3–xClx perovskite during thermal annealing using X-ray scattering Advanced Functional Materials, May 2016 DOI: 10.1002/adfm.201601309
Phase behavior of lysozyme solutions in the liquid–liquid phase coexistence region at high hydrostatic pressures Physical Chemistry Chemical Physics, May 2016 DOI: 10.1039/C6CP01791F
Journal Paper I22-Small angle scattering & Diffraction
Added alkane allows thermal thinning of supramolecular columns by forming superlattice - an X-ray and neutron study Journal Of The American Chemical Society, Apr 2016 DOI: 10.1021/jacs.6b01172
Journal Paper I22-Small angle scattering & Diffraction
In situ small-angle X-ray scattering studies of sterically-stabilized diblock copolymer nanoparticles formed during polymerization-induced self-assembly in non-polar media Chemical Science, Apr 2016 DOI: 10.1039/C6SC01243D
Micelle structure in a deep eutectic solvent: a small-angle scattering stud Physical Chemistry Chemical Physics, Apr 2016 DOI: 10.1039/C6CP01757F
Formation of calcium sulfate through the aggregation of sub-3 nanometre primary species Nature Communications, 7 Apr 2016 DOI: 10.1038/ncomms11177
Harnessing honeycombs Apr 2016
Science Highlight I16-Materials and Magnetism I22-Small angle scattering & Diffraction
Structure evolution in polyethylene terephthalate (PET) - multi-walled carbon nanotube (MWCNT) composite films during in-situ uniaxial deformation Polymer, Mar 2016 DOI: 10.1016/j.polymer.2016.03.071
Journal Paper I22-Small angle scattering & Diffraction
Ca-dependent folding of human calumenin Plos One, 11 Mar 2016 DOI: 10.1371/journal.pone.0151547
Journal Paper B21-High Throughput SAXS B23-Circular Dichroism I22-Small angle scattering & Diffraction open access
A novel polymeric prosthetic heart valve: design, manufacture, and testing Mar 2016 DOI: 10.17863/CAM.248
Thesis I22-Small angle scattering & Diffraction
Ultrastructural evaluation of pathological and acutely injured mammalian corneas Mar 2016
Thesis I02-Macromolecular Crystallography I22-Small angle scattering & Diffraction
Combined pressure and temperature denaturation of ribonuclease A produces alternate denatured states Biochemical And Biophysical Research Communications, Mar 2016 DOI: 10.1016/j.bbrc.2016.03.135
Journal Paper I22-Small angle scattering & Diffraction
Inducing structural changes in biological polymers Mar 2016
Thesis I22-Small angle scattering & Diffraction
Anti-reflective coatings based on diblock copolymer nanoparticles Feb 2016
Thesis I22-Small angle scattering & Diffraction
Structural characterization of twisted gastrulation provides insights into opposing functions on the BMP signalling pathway Matrix Biology, Jan 2016 DOI: 10.1016/j.matbio.2016.01.019
Heterogeneity of collagen VI microfibrils: structural analysis of non-collagenous regions Journal Of Biological Chemistry, Jan 2016 DOI: 10.1074/jbc.M115.705160
Use of commercial block copolymers as soot dispersants in engine oil Jan 2016
Thesis I22-Small angle scattering & Diffraction
How do spherical diblock copolymer nanoparticles grow during RAFT alcoholic dispersion polymerization? Macromolecules, 49 (1) Jan 2016 DOI: 10.1021/acs.macromol.5b02385
- Rogier Besselink, Tomasz Stawski, Alexander E. S. Van Driessche, Liane G Benning, "Not just fractal surfaces, but surface fractal aggregates: Derivation of the expression for the structure factor and its applications", The Journal Of Chemical Physics, 145 (2016), DOI: 10.1063/1.4960953
- Catherine R. Back, Maryta N. Sztukowska, Marisa Till, Richard J. Lamont, Howard F. Jenkinson, Angela H. Nobbs, Paul R. Race, "The Streptococcus gordonii adhesin CshA binds host fibronectin via a catch-clamp mechanism", Journal Of Biological Chemistry (2016), DOI: 10.1074/jbc.M116.760975
- Blandine Poulet, Ke Liu, Darren Plumb, Phoung Vo, Mittal Shah, Katherine Staines, Alexandra Sampson, Hiroyuki Nakamura, Hideaki Nagase, Alessandra Carriero, Sandra Shefelbine, Andrew A. Pitsillides, George Bou-Gharios, "Overexpression of TIMP-3 in chondrocytes produces transient reduction in growth plate length but permanently reduces adult bone quality and quantity", Plos One, 11 (2016), DOI: 10.1371/journal.pone.0167971
- [Book Chapter] Susanne Klein, Robert M. Richardson, Alexey Eremin, "Liquid crystalline phases in suspensions of pigments in non-polar solvents" (2016), DOI: 10.1142/9789814619264_0026
- [Thesis] Tomas White, "Structural studies of the corneal stroma with focus on the elastic fibre network in health and disease" (2016)
- C. J. Mable, K. L. Thompson, M. J. Derry, O. O. Mykhaylyk, B. P. Binks, S. P. Armes, "ABC triblock copolymer worms: synthesis, characterization, and evaluation as pickering emulsifiers for millimeter-sized droplets", Macromolecules, 49, 7897 - 7907 (2016), DOI: 10.1021/acs.macromol.6b01729
- Jingyi Mo, Sylvain F. Prévost, Liisa M. Blowes, Michaela Egertová, Nicholas J. Terrill, Wen Wang, Maurice R. Elphick, Himadri S. Gupta, "Interfibrillar stiffening of echinoderm mutable collagenous tissue demonstrated at the nanoscale", Proceedings Of The National Academy Of Sciences (2016), DOI: 10.1073/pnas.1609341113
- Gregory N. Smith, Samuel D. Finlayson, David Gillespie, Jocelyn Peach, Jonathan Pegg, Sarah Rogers, Olga Shebanova, Ann Terry, Steven P. Armes, Paul Bartlett, Julian Eastoe, "The internal structure of poly(methyl methacrylate) latexes in nonpolar solvents", Journal Of Colloid And Interface Science, 479, 234 - 243 (2016), DOI: 10.1016/j.jcis.2016.06.027
- Philippe Poulin, Rouhollah Jalili, Wilfrid Neri, Frederic Nallet, Thibaut Divoux, Annie Colin, Seyed Hamed Aboutalebi, Gordon Wallace, Cecile Zakri, "Superflexibility of graphene oxide", Proceedings Of The National Academy Of Sciences, 113, 11088 - 11093 (2016), DOI: 10.1073/pnas.1605121113
- Xiaohong Yao, Liliana Cseh, Xiangbing Zeng, Min Xue, Yongsong Liu, Goran Ungar, "Body-centred cubic packing of spheres – the ultimate thermotropic assembly mode for highly divergent dendrons", Nanoscale Horizons, 2, 43 - 49 (2016), DOI: 10.1039/C6NH00155F
- [Thesis] Li Xi, "Multiscale structure and mechanics of bone in glucocorticoid induced osteoporosis" (2016)
- [Thesis] Nutaporn Kamonsutthipaijit, "Self-assembly and template-directed synthesis in multi-strand porphyrin arrays" (2016)
- Micha Kornreich, Eti Malka-Gibor, Ben Zuker, Adi Laser-Azogui, Roy Beck, "Neurofilaments function as shock absorbers: compression response arising from disordered proteins", Physical Review Letters, 117 (2016), DOI: 10.1103/PhysRevLett.117.148101
- Rona Shaharabani, Maor Ram-On, Ram Avinery, Rina Aharoni, Ruth Arnon, Yeshayahu Talmon, Roy Beck, "Structural transition in myelin membrane as initiator of multiple sclerosis", Journal Of The American Chemical Society, 138, 12159 - 12165 (2016), DOI: 10.1021/jacs.6b04826
- [Thesis] Samuel J. Richardson, "Hard and soft nanomaterial films" (2016)
- [Thesis] Matthew Derry, "Polymerisation-induced self-assembly in non-polar solvents" (2016)
- Lucia Podhorska, Derfogail Delcassian, Angela Goode, Michael Agyei, David W. Mccomb, Mary Ryan, Iain Dunlop, "Mechanisms of polymer-templated nanoparticle synthesis: contrasting ZnS and Au", Langmuir (2016), DOI: 10.1021/acs.langmuir.6b01900
- Joshua Weatherill, Katherine Morris, Pieter Bots, Tomasz Stawski, Arne Janssen, Liam Abrahamsen, Richard Blackham, Sam Shaw, "Ferrihydrite formation: the role of Fe13 Keggin clusters", Environmental Science & Technology (2016), DOI: 10.1021/acs.est.6b02481
- Fabio Bianchi, Felix Hofmann, Andrew J. Smith, Mark S. Thompson, "Probing multi-scale mechanical damage in connective tissues using x-ray diffraction", Acta Biomaterialia (2016), DOI: 10.1016/j.actbio.2016.08.027
- Martin Alfred Schroer, Florian Schulz, Felix Lehmkühler, Johannes Möller, Andrew J. Smith, Holger Lange, Tobias Vossmeyer, Gerhard Grübel, "Tuning the interaction of nanoparticles from repulsive to attractive by pressure", The Journal Of Physical Chemistry C (2016), DOI: 10.1021/acs.jpcc.6b06847
- [Diamond Annual Review Highlight] Diamond Light Source, "Making gold metamaterials with a twist" (2016)
- [Diamond Annual Review Highlight] Diamond Light Source, "Hybrid glasses: A new family of glasses captured with small angle X-ray scattering and calorimetry" (2016)
- Bernice Akpinar, Lee Fielding, Victoria J. Cunningham, Yin Ning, Oleksandr Mykhaylyk, Patrick W. Fowler, Steven P. Armes, "Determining the effective density and stabilizer layer thickness of sterically stabilized nanoparticles", Macromolecules (2016), DOI: 10.1021/acs.macromol.6b00987
- Martin J. Hollamby, Keisuke Aratsu, B R. Pauw, Sarah Rogers, Andrew J. Smith, Mitsuaki Yamauchi, Xu Lin, Shiki Yagai, "Simultaneous SAXS and SANS analysis for the detection of toroidal supramolecular polymers composed of noncovalent supermacrocycles in solution", Angewandte Chemie International Edition (2016), DOI: 10.1002/anie.201603370
- Florian Schulz, Gregor T. Dahl, Stephanie Besztejan, Martin Alfred Schroer, Felix Lehmkühler, Gerhard Grübel, Tobias Vossmeyer, Holger Lange, "Ligand layer engineering to control stability and interfacial properties of nanoparticles", Langmuir (2016), DOI: 10.1021/acs.langmuir.6b01704
- [Science Highlight] Diamond Light Source, "Understanding gypsum growth" (2016)
- Charlotte Beddoes, Johanna Berge, Julia Bartenstein, Kathrin Lange, Andrew J. Smith, Richard K. Heenan, Wuge H. Briscoe, "Hydrophilic nanoparticles stabilising mesophase curvature at low concentration but disrupting mesophase order at higher concentrations", Soft Matter (2016), DOI: 10.1039/C6SM00393A
- Xiangbing Zeng, Marko Prehm, Goran Ungar, Carsten Tschierske, Feng Liu, "Formation of a double diamond cubic phase by thermotropic liquid crystalline self-assembly of bundled bolaamphiphiles", Angewandte Chemie International Edition (2016), DOI: 10.1002/anie.201602734
- Andreas S. Poulos, Manuela Nania, Paul Lapham, Ruhina Miller, Andrew J. Smith, Hossam Tantawy, Joel Caragay, Jérémie Gummel, Oscar Ces, Eric S. J. Robles, Joao Cabral, "Microfluidic SAXS study of lamellar and multilamellar vesicle phases of linear sodium alkylbenzenesulfonate surfactant with intrinsic isomeric distribution", Langmuir, 32 (23), 5852–5861 (2016), DOI: 10.1021/acs.langmuir.6b01240
- D. Hayward, G. Whittell, J. Gilroy, I. Manners, R. M Richardson, "An investigation into the hexagonal phases formed in high-concentration dispersions of well-defined cylindrical block copolymer micelles", Liquid Crystals (2016), DOI: 10.1080/02678292.2016.1170217
- Y. Zhang, O. Paris, N. J. Terrill, H. Gupta, "Uncovering three-dimensional gradients in fibrillar orientation in an impact-resistant biological armour", Scientific Reports, 6 (2016), DOI: 10.1038/srep26249
- Alex Barrows, Samuele Lilliu, Andrew Pearson, David Babonneau, Alan Dunbar, David Lidzey, "Monitoring the formation of a CH3NH3PbI3–xClx perovskite during thermal annealing using X-ray scattering", Advanced Functional Materials (2016), DOI: 10.1002/adfm.201601309
- Julian Schulze, Johannes Möller, Jonathan Weiner, Karin Julius, Nico König, Julia Nase, Michael Paulus, Metin Tolan, Roland Winter, "Phase behavior of lysozyme solutions in the liquid–liquid phase coexistence region at high hydrostatic pressures", Physical Chemistry Chemical Physics (2016), DOI: 10.1039/C6CP01791F
- Ming-Huei Yen, Jitrin Chaiprapa, Xiangbing Zeng, Yongsong Liu, Liliana Cseh, Georg H. Mehl, Goran Ungar, "Added alkane allows thermal thinning of supramolecular columns by forming superlattice - an X-ray and neutron study", Journal Of The American Chemical Society (2016), DOI: 10.1021/jacs.6b01172
- Matthew Derry, Lee Fielding, Nicholas Warren, Charlotte Mable, Andrew J Smith, Oleksandr Mykhaylyk, Steven P. Armes, "In situ small-angle X-ray scattering studies of sterically-stabilized diblock copolymer nanoparticles formed during polymerization-induced self-assembly in non-polar media", Chemical Science (2016), DOI: 10.1039/C6SC01243D
- Adrian Sanchez Fernandez, Karen J. Edler, Tom Arnold, Richard K Heenan, Lionel Porcar, Nicholas Terrill, Ann Terry, Andrew Jackson, "Micelle structure in a deep eutectic solvent: a small-angle scattering stud", Physical Chemistry Chemical Physics (2016), DOI: 10.1039/C6CP01757F
- Tomasz Stawski, Alexander E. S. Van Driessche, Mercedes Ossorio, Juan Diego Rodriguez-Blanco, Rogier Besselink, Liane G Benning, "Formation of calcium sulfate through the aggregation of sub-3 nanometre primary species", Nature Communications, 7 (2016), DOI: 10.1038/ncomms11177
- [Science Highlight] Diamond Light Source, "Harnessing honeycombs" (2016)
- Ellen L. Heeley, Darren J. Hughes, Eleanor Crabb, Matthew Kershaw, Olga Shebanova, Sandy Leung, Tony Mcnally, "Structure evolution in polyethylene terephthalate (PET) - multi-walled carbon nanotube (MWCNT) composite films during in-situ uniaxial deformation", Polymer (2016), DOI: 10.1016/j.polymer.2016.03.071
- Marco Mazzorana, Rohanah Hussain, Thomas Sorensen, "Ca-dependent folding of human calumenin", Plos One, 11 (2016), DOI: 10.1371/journal.pone.0151547
- [Thesis] Jacob Brubert, "A novel polymeric prosthetic heart valve: design, manufacture, and testing" (2016), DOI: 10.17863/CAM.248
- [Thesis] Erin P. Dooley, "Ultrastructural evaluation of pathological and acutely injured mammalian corneas" (2016)
- Timothy M. Ryan, Yun Xun, Nathan P. Cowieson, Jitendra P. Mata, Andrew Jackson, Brian R. Pauw, Andrew Smith, Nigel Kirby, Duncan Mcgillivray, "Combined pressure and temperature denaturation of ribonuclease A produces alternate denatured states", Biochemical And Biophysical Research Communications (2016), DOI: 10.1016/j.bbrc.2016.03.135
- [Thesis] Joanna Glab, "Inducing structural changes in biological polymers" (2016)
- [Thesis] Elizabeth Jones, "Anti-reflective coatings based on diblock copolymer nanoparticles" (2016)
- Helen Troilo, Anne L. Barrett, Alexandra V. Zuk, Michael P. Lockhart-Cairns, Alexander P. Wohl, Christopher Bayley, Rana Dajani, Richard Tunnicliffe, Lewis Green, Thomas A. Jowitt, Gerhard Sengle, Clair Baldock, "Structural characterization of twisted gastrulation provides insights into opposing functions on the BMP signalling pathway", Matrix Biology (2016), DOI: 10.1016/j.matbio.2016.01.019
- Tobias Maaß, Christopher P Bayley, Matthias Mörgelin, Sandra Lettmann, Paolo Bonaldo, Mats Paulsson, Clair Baldock, Raimund Wagener, "Heterogeneity of collagen VI microfibrils: structural analysis of non-collagenous regions", Journal Of Biological Chemistry (2016), DOI: 10.1074/jbc.M115.705160
- [Thesis] D. Growney, "Use of commercial block copolymers as soot dispersants in engine oil" (2016)
- E. R. Jones, O. O. Mykhaylyk, M. Semsarilar, M. Boerakker, P. Wyman, S. P. Armes, "How do spherical diblock copolymer nanoparticles grow during RAFT alcoholic dispersion polymerization?", Macromolecules, 49 (1), 172 - 181 (2016), DOI: 10.1021/acs.macromol.5b02385
Beamline Technical Publications
Diamond Light Source is the UK's national synchrotron science facility, located at the Harwell Science and Innovation Campus in Oxfordshire.
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Oxfordshire
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