Instruments by Science Group
Macromolecular
Soft Condensed 
Imaging and
Biological
Magnetic
Structures and
Crystallography 
Spectroscopy I22 Contact
Beamline phone numbers:
+44 (0) 1235 77 8617
+44 (0) 1235 77 8713
Principal Beamline Scientist:
Nick Terrill
Tel: +44 (0) 1235 778047
E-mail: [email protected]
Science Group Leader
Robert Rambo
Email: [email protected]
Tel: +44 (0)1235 56 7675
Beamline Paper
We have just published a Review of I22 Operations. It contains a description of beamline. As part of the requirement to include Diamond in your publication acknowledgements and references please include this paper for all work carried out on I22. We hope you find it useful.
User Publications
These papers are all based at least in part on data gathered on beamline I22. If you have published a paper based on data from I22 which doesn't appear here, please send a reference (ideally including a DOI) to us.
38 items found for 2012 [total: 740]
Effects of tensile strain on the nanostructure of irradiated and thermally stabilised ultra high molecular weight polyethylenes for orthopaedic devices Rsc Advances, Dec 2012 DOI: 10.1039/c2ra21722h
Journal Paper I22-Small angle scattering & Diffraction
Fibrillin-1 mutations causing Weill-Marchesani syndrome and Acromicric and Geleophysic Dysplasias disrupt heparan sulfate interactions Plos One, 7 (11) Nov 2012 DOI: 10.1371/journal.pone.0048634
In situ beamline analysis and correction of active optics Journal Of Synchrotron Radiation, 19 (6) Nov 2012 DOI: 10.1107/S090904951203662X
Journal Paper I02-Macromolecular Crystallography I03-Macromolecular Crystallography I04-Macromolecular Crystallography I15-Extreme Conditions I19-Small Molecule Single Crystal Diffraction I20-Scanning-X-ray spectroscopy (XAS/XES) I22-Small angle scattering & Diffraction
Fractionated crystallization of defect-free poly(3-hexylthiophene) Acs Macro Letters, 1 (10) Oct 2012 DOI: 10.1021/mz3003769
Journal Paper I22-Small angle scattering & Diffraction
Arrays of giant octagonal and square cylinders by liquid crystalline self-assembly of X-shaped polyphilic molecules Nature Communications, 3 Oct 2012 DOI: 10.1038/ncomms2096
Characterizing size and porosity of hollow nanoparticles: SAXS, SANS, TEM, DLS, and adsorption isotherms compared Langmuir, 28 (43) Oct 2012 DOI: 10.1021/la302236u
Hydrostatic pressure effects on the lamellar to gyroid cubic phase transition of monolinolein at limited hydration Langmuir, 28 (36) Sept 2012 DOI: 10.1021/la3025843
Journal Paper I22-Small angle scattering & Diffraction
Structure and optical function of amorphous photonic nanostructures from avian feather barbs: a comparative small angle X-ray scattering (SAXS) analysis of 230 bird species Journal Of The Royal Society Interface, 9 (75) Aug 2012 DOI: 10.1098/rsif.2012.0191
Journal Paper I22-Small angle scattering & Diffraction
Self-organization of bent rod molecules into hexagonally ordered vesicular columns Journal Of The American Chemical Society, 134 (33) Aug 2012 DOI: 10.1021/ja3060904
Journal Paper I22-Small angle scattering & Diffraction
Coassembly of poly(ethylene oxide)-block-poly(methacrylic acid) and N-dodecylpyridinium chloride in aqueous solutions leading to ordered micellar assemblies within copolymer aggregates Macromolecules, 45 (16) Aug 2012 DOI: 10.1021/ma301510j
Journal Paper I22-Small angle scattering & Diffraction
Nematic director-induced switching of assemblies of hexagonally packed gold nanorods Advanced Materials, 24 (32) Aug 2012 DOI: 10.1002/adma.201201319
Journal Paper I22-Small angle scattering & Diffraction
HATSAXS : a versatile high-throughput system for solution SAXS Jul 2012
Thesis I22-Small angle scattering & Diffraction
Large multimeric assemblies of nucleosome assembly protein and histones revealed by small-angle X-ray scattering and electron microscopy Journal Of Biological Chemistry, June 2012 DOI: 10.1074/jbc.M112.340422
Silica-surfactant-polyelectrolyte film formation: evolution in the subphase Langmuir, 28 (22) June 2012 DOI: 10.1021/la3014317
Journal Paper I22-Small angle scattering & Diffraction
The low-resolution solution structure of Vibrio cholerae Hfq in complex with Qrr1 sRNA Nucleic Acids Research, June 2012 DOI: 10.1093/nar/gks582
Understanding the basis of corneal shape and transparency June 2012
Thesis I02-Macromolecular Crystallography I22-Small angle scattering & Diffraction
Quantitative assessment of ultrastructure and light scatter in mouse corneal debridement wounds Investigative Ophthalmology & Visual Science, 53 (6) May 2012 DOI: 10.1167/iovs.11-9305
Journal Paper I22-Small angle scattering & Diffraction
Disruption in fibrillar level fracture mechanisms in rachitic mice bone: Measured using in-situ cantilever bending with microfocus saxd Bone, 50 May 2012 DOI: 10.1016/j.bone.2012.02.381
Poster I22-Small angle scattering & Diffraction
Synthesis, purification, and characterization of well-defined all-conjugated diblock copolymers PF8TBT-b-P3HT Macromolecules, 45 (10) May 2012 DOI: 10.1021/ma300533k
Journal Paper I22-Small angle scattering & Diffraction
One-step synthesis and self-assembly of metal oxide nanoparticles into 3D superlattices Acs Nano, 6 (5) May 2012 DOI: 10.1021/nn3010735
Journal Paper I22-Small angle scattering & Diffraction
Mechanistic insights into the crystallization of amorphous calcium carbonate (ACC) Crystal Growth & Design, 12 (7) May 2012 DOI: 10.1021/cg300676b
Journal Paper I22-Small angle scattering & Diffraction
Experimental investigation of calcium carbonate mineralogy in past and future oceans May 2012
Thesis I22-Small angle scattering & Diffraction
Hypophosphatemic rickets is associated with disruption of mineral orientation at the nanoscale in the flat scapula bones of rachitic mice with development Bone, Apr 2012 DOI: 10.1016/j.bone.2012.04.021
Aggregation and settling in aqueous polydisperse alumina nanoparticle suspensions Journal Of Nanoparticle Research, 14 (851) Apr 2012 DOI: 10.1007/s11051-012-0851-3
Journal Paper I22-Small angle scattering & Diffraction
Control of anisotropic self-assembly of gold nanoparticles coated with mesogens Journal Of Materials Chemistry, 22 (22) Apr 2012 DOI: 10.1039/c2jm16794h
Journal Paper I22-Small angle scattering & Diffraction
Correlating structure with optoelectronic functionality in polymer:fullerene blend films Apr 2012
Thesis I07-Surface & interface diffraction I22-Small angle scattering & Diffraction open access
Analysis of alterations in matrix quality at nanoscale in metabolic bone diseases using synchrotron X-ray diffraction Apr 2012
Thesis I22-Small angle scattering & Diffraction
On the role of single regiodefects and polydispersity in regioregular poly(3-hexylthiophene): defect distribution, synthesis of defect-free chains, and a simple model for the determination of crystallinity Journal Of The American Chemical Society, 134 (10) Mar 2012 DOI: 10.1021/ja210871j
Journal Paper I22-Small angle scattering & Diffraction
Significant deterioration in nanomechanical quality occurs through incomplete extrafibrillar mineralization in rachitic bone: evidence from in-situ synchrotron X-ray scattering and backscattered electron imaging Journal Of Bone And Mineral Research, 27 (4) Mar 2012 DOI: 10.1002/jbmr.1495
Journal Paper I22-Small angle scattering & Diffraction
Effects of isopropanol on collagen fibrils in new parchment Chemistry Central Journal, 6 Mar 2012 DOI: 10.1186/1752-153X-6-24
Crystal morphology of strained ultra high molecular weight polyethylenes Polymer Testing, 31 (5) Mar 2012 DOI: 10.1016/j.polymertesting.2012.03.009
Journal Paper I22-Small angle scattering & Diffraction
SAXS study of sterically stabilized lipid nanocarriers functionalized by DNA Journal of Physics: Conference Series, 351 Mar 2012 DOI: 10.1088/1742-6596/351/1/012004
3D Micro- and nanostructural analysis of connective tissue in the human optic nerve head (ONH) Mar 2012
Conference Paper I22-Small angle scattering & Diffraction
Pressure-temperature phase behaviour of natural sphingomyelin extracts Soft Matter, 8 (4) Jan 2012 DOI: 10.1039/c1sm06703f
Journal Paper I22-Small angle scattering & Diffraction
Formation of shear thinning gels from partially oxidised cellulose nanofibrils Green Chemistry, 14 (2) Jan 2012 DOI: 10.1039/c2gc16302k
Journal Paper I22-Small angle scattering & Diffraction
Synthesis, alignment, and magnetic properties of monodisperse nickel nanocubes Journal Of The American Chemical Society, 134 (2) Jan 2012 DOI: 10.1021/ja210209r
Journal Paper I22-Small angle scattering & Diffraction
Induction of thermotropic bicontinuous cubic phases in liquid-crystalline ammonium and phosphonium salts Journal Of The American Chemical Society, 134 (5) Jan 2012 DOI: 10.1021/ja209010m
Journal Paper I22-Small angle scattering & Diffraction
Small-angle X-ray scattering investigations of biomolecular confinement, loading, and release from liquid-crystalline nanochannel assemblies The Journal Of Physical Chemistry Letters, 3 (3) Jan 2012 DOI: 10.1021/jz2014727
Journal Paper I22-Small angle scattering & Diffraction
- M. N. Collins, E. Dalton, J. J. Leahy, C. Birkinshaw, "Effects of tensile strain on the nanostructure of irradiated and thermally stabilised ultra high molecular weight polyethylenes for orthopaedic devices", Rsc Advances (2012), DOI: 10.1039/c2ra21722h
- Stuart A. Cain, Amanda Mcgovern, Andrew K. Baldwin, Clair Baldock, Cay M. Kielty, "Fibrillin-1 mutations causing Weill-Marchesani syndrome and Acromicric and Geleophysic Dysplasias disrupt heparan sulfate interactions", Plos One, 7 (11) (2012), DOI: 10.1371/journal.pone.0048634
- John Sutter, Simon Alcock, Kawal Sawhney, "In situ beamline analysis and correction of active optics", Journal Of Synchrotron Radiation, 19 (6), 960 - 968 (2012), DOI: 10.1107/S090904951203662X
- P. Kohn, U. Steiner, M. Sommer, S. Huettner, "Fractionated crystallization of defect-free poly(3-hexylthiophene)", Acs Macro Letters, 1 (10), 1170 - 1175 (2012), DOI: 10.1021/mz3003769
- Feng Liu, Robert Kieffer, Xiangbing Zeng, Karsten Pelz, Marko Prehm, Goran Ungar, Carsten Tschierske, "Arrays of giant octagonal and square cylinders by liquid crystalline self-assembly of X-shaped polyphilic molecules", Nature Communications, 3, 2563-2580 (2012), DOI: 10.1038/ncomms2096
- Zhi Hong Chen, Chanhoi Kim, Xiang-Bing Zeng, Sun Hye Hwang, Jyongsik Jang, Goran Ungar, "Characterizing size and porosity of hollow nanoparticles: SAXS, SANS, TEM, DLS, and adsorption isotherms compared", Langmuir, 28 (43), 15350 - 15361 (2012), DOI: 10.1021/la302236u
- T.-Y. Dora Tang, Nicholas J. Brooks, Christoph Jeworrek, Oscar Ces, Nicholas Terrill, Roland Winter, Richard H. Templer, John Seddon, "Hydrostatic pressure effects on the lamellar to gyroid cubic phase transition of monolinolein at limited hydration", Langmuir, 28 (36), 13018 - 13024 (2012), DOI: 10.1021/la3025843
- Vinod Kumar Saranathan, Jason Forster, Heeso Noh, Seng-Fatt Liew, Simon Mochrie, Hui Cao, Eric Dufresne, Richard Prum, "Structure and optical function of amorphous photonic nanostructures from avian feather barbs: a comparative small angle X-ray scattering (SAXS) analysis of 230 bird species", Journal Of The Royal Society Interface, 9 (75), 11101-11106 (2012), DOI: 10.1098/rsif.2012.0191
- Ho-Joong Kim, Feng Liu, Ja-Hyoung Ryu, Seong-Kyun Kang, Xiangbing Zeng, Goran Ungar, Jeong-Kyu Lee, Wang-Cheol Zin, Myongsoo Lee, "Self-organization of bent rod molecules into hexagonally ordered vesicular columns", Journal Of The American Chemical Society, 134 (33), 13871 - 13880 (2012), DOI: 10.1021/ja3060904
- Mariusz Uchman, Miroslav Stěpánek, Sylvain Prévost, Borislav Angelov, Jan Bednár, Marie-Sousai Appavou, Michael Gradzielski, Karel Procházka, "Coassembly of poly(ethylene oxide)-block-poly(methacrylic acid) and N-dodecylpyridinium chloride in aqueous solutions leading to ordered micellar assemblies within copolymer aggregates", Macromolecules, 45 (16), 6471 - 6480 (2012), DOI: 10.1021/ma301510j
- Michael R. Thomas, Susanne Klein, Robert Greasty, Stephen Mann, Adam W. Perriman, Robert M. Richardson, "Nematic director-induced switching of assemblies of hexagonally packed gold nanorods", Advanced Materials, 24 (32), 4424 - 4429 (2012), DOI: 10.1002/adma.201201319
- [Thesis] Gudrun Lotze, "HATSAXS : a versatile high-throughput system for solution SAXS" (2012)
- E. R. Newman, G. G. Kneale, R. B. G. Ravelli, M. Karuppasamy, F. K. Nejadasl, I. A. Taylor, J. E. Mcgeehan, "Large multimeric assemblies of nucleosome assembly protein and histones revealed by small-angle X-ray scattering and electron microscopy", Journal Of Biological Chemistry (2012), DOI: 10.1074/jbc.M112.340422
- Bin Yang, Robben Jaber, Karen J. Edler, "Silica-surfactant-polyelectrolyte film formation: evolution in the subphase", Langmuir, 28 (22), 8337 - 8347 (2012), DOI: 10.1021/la3014317
- H. A. Vincent, C. A. Henderson, C. M. Stone, P. D. Cary, D. M. Gowers, F. Sobott, J. E. Taylor, A. J. Callaghan, "The low-resolution solution structure of Vibrio cholerae Hfq in complex with Qrr1 sRNA", Nucleic Acids Research (2012), DOI: 10.1093/nar/gks582
- [Thesis] Patrycja Joanna Boguslawska, "Understanding the basis of corneal shape and transparency" (2012)
- C. Boote, Y. Du, S. Morgan, J. Harris, C. S. Kamma-Lorger, S. Hayes, K. L. Lathrop, D. S. Roh, M. K. Burrow, J. Hiller, N. J. Terrill, J. L. Funderburgh, K. M. Meek, "Quantitative assessment of ultrastructure and light scatter in mouse corneal debridement wounds", Investigative Ophthalmology & Visual Science, 53 (6), 2786 - 2795 (2012), DOI: 10.1167/iovs.11-9305
- [Poster] A. Karunaratne, C. Esapa, J. Hiller, N. Terrill, S. Brown, R. Cox, R. Thakker, H. Gupta, "Disruption in fibrillar level fracture mechanisms in rachitic mice bone: Measured using in-situ cantilever bending with microfocus saxd", Bone, 50, S123 (2012), DOI: 10.1016/j.bone.2012.02.381
- Michael Sommer, Hartmut Komber, Rhiannon Mulherin, Peter Kohn, Neil C. Greenham, Wilhelm T. S. Huck, Sven Huettner, "Synthesis, purification, and characterization of well-defined all-conjugated diblock copolymers PF8TBT-b-P3HT", Macromolecules, 45 (10), 4142 - 4151 (2012), DOI: 10.1021/ma300533k
- Andrea Pucci, Marc-Georg Willinger, Feng Liu, Xiangbing Zeng, Valentina Rebuttini, Guylhaine Clavel, Xue Bai, Goran Ungar, Nicola Pinna, "One-step synthesis and self-assembly of metal oxide nanoparticles into 3D superlattices", Acs Nano, 6 (5), 4382 - 4391 (2012), DOI: 10.1021/nn3010735
- Pieter Bots, Liane G. Benning, Juan Diego Rodriguez Blanco, Teresa Roncal-Herrero, Samuel Shaw, "Mechanistic insights into the crystallization of amorphous calcium carbonate (ACC)", Crystal Growth & Design, 12 (7) (2012), DOI: 10.1021/cg300676b
- [Thesis] Pieter Bots, "Experimental investigation of calcium carbonate mineralogy in past and future oceans" (2012)
- A. Karunaratne, G. R. Davis, J. Hiller, C. T. Esapa, N. J. Terrill, S. D. M. Brown, R. D. Cox, R. V. Thakker, H. S. Gupta, "Hypophosphatemic rickets is associated with disruption of mineral orientation at the nanoscale in the flat scapula bones of rachitic mice with development", Bone (2012), DOI: 10.1016/j.bone.2012.04.021
- Sanjeeva Witharana, Chris Hodges, Dan Xu, Xiaojun Lai, Yulong Ding , "Aggregation and settling in aqueous polydisperse alumina nanoparticle suspensions", Journal Of Nanoparticle Research, 14 (851), 14 (851) (2012), DOI: 10.1007/s11051-012-0851-3
- Xiaobin Mang, Xiangbing Zeng, Baijia Tang, Feng Liu, Goran Ungar, Ruibin Zhang, Liliana Cseh, Georg H. Mehl, "Control of anisotropic self-assembly of gold nanoparticles coated with mesogens", Journal Of Materials Chemistry, 22 (22) (2012), DOI: 10.1039/c2jm16794h
- [Thesis] Andrew Pearson, "Correlating structure with optoelectronic functionality in polymer:fullerene blend films" (2012)
- [Thesis] Malintha P. Angelo Karunaratne, "Analysis of alterations in matrix quality at nanoscale in metabolic bone diseases using synchrotron X-ray diffraction" (2012)
- Peter Kohn, Hartmut Komber, Volodymyr Senkovskyy, Roman Tkachov, Anton Kiriy, Richard H. Friend, Ullrich Steiner, Wilhelm T. S. Huck, Jens-Uwe Sommer, Michael Sommer, Sven Huettner, "On the role of single regiodefects and polydispersity in regioregular poly(3-hexylthiophene): defect distribution, synthesis of defect-free chains, and a simple model for the determination of crystallinity", Journal Of The American Chemical Society, 134 (10), 4790 - 4805 (2012), DOI: 10.1021/ja210871j
- Malintha Karunaratne, Christopher R. Esapa, Jennifer Hiller, Alan Boyde, Rosie Head, J. H. Duncan Bassett, Nicholas J. Terrill, Graham R. Williams, Matthew A. Brown, Peter I. Croucher, Steve D. M. Brown, Roger D. Cox, Rajesh V. Thakker, Himadri Sh. Gupta, Asa Barber, "Significant deterioration in nanomechanical quality occurs through incomplete extrafibrillar mineralization in rachitic bone: evidence from in-situ synchrotron X-ray scattering and backscattered electron imaging", Journal Of Bone And Mineral Research, 27 (4) (2012), DOI: 10.1002/jbmr.1495
- Lee G. Gonzalez, Jennifer Hiller, Nick J. Terrill, Joanna Parkinson, Kate Thomas, Tim J. Wess, "Effects of isopropanol on collagen fibrils in new parchment", Chemistry Central Journal, 6, 24 (2012), DOI: 10.1186/1752-153X-6-24
- Maurice N. Collins, Eric Dalton, Barbara Schaller, J. J. Leahy, Colin Birkinshaw, "Crystal morphology of strained ultra high molecular weight polyethylenes", Polymer Testing, 31 (5), 629 - 637 (2012), DOI: 10.1016/j.polymertesting.2012.03.009
- [Conference Paper] Borislav Angelov, Angelina Angelova, Sergey Filippov, Göran Karlsson, Nicholas Terrill, Sylviane Lesieur, Petr Stepanek, "SAXS study of sterically stabilized lipid nanocarriers functionalized by DNA", Journal of Physics: Conference Series, 351 (2012), DOI: 10.1088/1742-6596/351/1/012004
- [Conference Paper] Hannah Jones, Nick White, Jennifer Hiller, Nicholas Terrill, Keith Meek, Craig Boote, Julie Albon, "3D Micro- and nanostructural analysis of connective tissue in the human optic nerve head (ONH)" (2012)
- Karen P. Shaw, Nicholas J. Brooks, James A. Clarke, Oscar Ces, John M. Seddon, Robert V. Law, "Pressure-temperature phase behaviour of natural sphingomyelin extracts", Soft Matter, 8 (4), 1070-1078 (2012), DOI: 10.1039/c1sm06703f
- Robert J. Crawford, Karen J. Edler, Saskia Lindhoud, Janet L. Scott, Gianfranco Unali, "Formation of shear thinning gels from partially oxidised cellulose nanofibrils", Green Chemistry, 14 (2), 300-303 (2012), DOI: 10.1039/c2gc16302k
- Alec P. Lagrow, Bridget Ingham, Soshan Cheong, Grant V. M. Williams, Christian Dotzler, Michael F. Toney, David A. Jefferson, Elena C. Corbos, Peter T. Bishop, James Cookson, Richard D. Tilley, "Synthesis, alignment, and magnetic properties of monodisperse nickel nanocubes", Journal Of The American Chemical Society, 134 (2), 855 - 858 (2012), DOI: 10.1021/ja210209r
- Takahiro Ichikawa, Masafumi Yoshio, Atsushi Hamasaki, Satomi Taguchi, Feng Liu, Xiang-Bing Zeng, Goran Ungar, Hiroyuki Ohno, Takashi Kato, "Induction of thermotropic bicontinuous cubic phases in liquid-crystalline ammonium and phosphonium salts", Journal Of The American Chemical Society, 134 (5) (2012), DOI: 10.1021/ja209010m
- Angelina Angelova, Borislav Angelov, Vasil M. Garamus, Patrick Couvreur, Sylviane Lesieur, "Small-angle X-ray scattering investigations of biomolecular confinement, loading, and release from liquid-crystalline nanochannel assemblies", The Journal Of Physical Chemistry Letters, 3 (3), 445-457 (2012), DOI: 10.1021/jz2014727
Beamline Technical Publications
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