Preparing for Beamtime
To be able to use your beamtime, a few things need to be done beforehand.
UAS (User Admininstration System)
- Make sure your PI has completed the safety paperwork in UAS.
- Make sure you are a registered user (with FedID and password). Please check that you are fully registered and complete any missing information.
- Ensure that you have been added to the session and check travel and accommodation.
- Ensure that investigators coming to Diamond have completed the online safety training within UAS, and follow any further advice from the User office.
Samples and experiment
- Talk to your local contact to discuss any experiment requirements.
- Prepare your samples in SPINE pins, Unipucks or the correct type of SBS plate.
Time Line for MX Experiments at Diamond Light Source
When | Who | Action | Tools |
3-6 months before | PI | Registers samples as part of beamtime application. |
|
> 2weeks before | PI |
Registers users and any extra samples OR cancel shift if you can’t use it. |
OR email [email protected] for cancellation |
> 1 week before | Users | Check necessary requirements all in place to conduct experiment and test connection to nx.diamond.ac.uk. | Remote Access |
> 4 days before | Users | Prepare shipping dewar including shipping information in ISPyB and prints labels. Use matched number Unipuck bases and lids. |
|
> 3 working days before | Users | Ship ISPyB labelled dewars to Diamond including return label with shipment. |
|
> 1 day before | Users | Should have received notification of arrival of dewar at Diamond. If no notification check dewar tracking with courier and ISPyB. | http://ispyb.diamond.ac.uk |
> 1 day before | Users | Upload samples in ISPyB. |
|
> 1 day before
|
Users | Browse MX website and check the beamline page. If any questions call or e-mail your local contact (LC). |
|
> 1 hour before | Users | Login using No Machine (NX). | Remote Access |
< 2 - 0 hours | LC/EHC | Will contact user to inform beamline available. | GDA messenger/ Email to user |
0 - 8 hours | Users |
Run experiments. If you finish early, call LC/EHC. |
01235 778787(EHC) or contact number LC provided you with |
8 hours | Users | Complete experiments, unload last sample and make hutch safe. | |
> 8 hours | Users/LC/EHC | Remove samples and put in storage dewar and attach included return label for return shipment. | |
Prior to and up to 1 day after | Users | Request dewar back. | Shipping Your Dewar Home |
> 1 day | Diamond Stores | Dewar collected by shipping company. | |
> 1 day | Users | Complete feedback form sent by the User office. | UAS |
> 2 days | Users | Dewar received | |
> 2 days | Users | If eligilble claim appropriate academic use costs from diamond |