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Crystallography
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Instruments by Science Group

Macromolecular
Crystallography
Soft Condensed
Matter
Imaging and
Microscopy
Biological
Cryo-Imaging
Magnetic
Materials
Structures and
Surfaces
Crystallography
Spectroscopy

I19 Contact

Beamline Phone Number:
+44 (0) 1235 778418

Principal Beamline Scientist: 
Dave Allan

Tel: +44 (0) 1235 778644
E-mail: [email protected]

More

Science Group Leader

Philip Chater

Email: [email protected]
Tel: +44 (0)1235 778677

I19 Small Molecule Single Crystal Diffraction

Status: Operational

Wavelength: 0.5 - 2.5 Å
Energy: 5 - 25 keV

Small Molecule Diffraction High Pressure Gas Environments X-ray Single Crystal Diffraction Humidity Control In situ Remote Access
  1. Instruments
  2. Crystallography
  3. I19
  4. Manuals
  5. EH1
  6. Preparation for Beamtime
  7. Assign Pucks

Assign Pucks

ISPyB

If not assigned by beamline staff, check the white board at the back of the hutch (webcam-11) to see where the pucks have been placed in the Dewars.

In ISPyB, click on Assign Containers, from the list

assign containers

Click on the current visit from the potential list

assign containers for a selected visit

This will take you to the page where all available puck positions are shown.

Note positions 1-7 are in Dewar 1 and 8-14 are in Dewar 2.

The pucks are listed in the appropriate shipment and all shipments associated with the visit should be shown.

Click on the puck and drag it to the correct position in the Dewars.  Click Ok to confirm the container assignment.  If you mis-place a puck, just drag the puck to the correct place and click Ok to confirm its new position.

Allocating pucks

Pucks assigned in ISPyB:

Pucks assigned

GDA

In the GDA – click on the Samples tab.  You may need to click on the Refresh button to update the list if the GDA was opened before the pucks were assigned to their locations.

Samples in sample changer tab

Please Note: Pucks for any given visit will normally all be placed in one Dewar, but sometimes they will be split between the 2 Dewars.  It is recommended to work through the pucks in one Dewar, unload the last sample (to force a gripper dry) and then work through the pucks in the other Dewar.  Measures in place to ensure the robot doesn’t drive through the side of the Dewar when moving from one Dewar to the other, mean the robot briefly sits at the wait position and then re-soaks in the new Dewar if you go directly from one to the other – there is a higher risk of icing doing it this way.

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Diamond Light Source

Diamond Light Source is the UK's national synchrotron science facility, located at the Harwell Science and Innovation Campus in Oxfordshire.

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