Instruments by Science Group
Macromolecular
Soft Condensed 
Imaging and
Biological
Magnetic
Structures and
Crystallography 
Spectroscopy B22 Contact
Beamline Phone Number:
+44 (0) 1235 778684
Principal Beamline Scientist:
Dr Gianfelice Cinque
Tel: +44 (0) 1235 778410
E-mail: [email protected]
Science Group Leader
Robert Rambo
Email: [email protected]
Tel: +44 (0)1235 56 7675
B22 Multimode InfraRed Imaging And Microspectroscopy
Status: Operational
Beamsize: 15µm to 3 µm by microFTIR; resolution 10 to 100 nm by nanoIR (s-SNOM & AFM IR)
Detector: MCT, FPA, DLaTGS and Bolometer
Wavelength: 1 mm - 1 µm (10,000 to 10 cm-1)
Energy: 1 meV - 1 eV
Detector: MCT, FPA, DLaTGS and Bolometer
Wavelength: 1 mm - 1 µm (10,000 to 10 cm-1)
Energy: 1 meV - 1 eV
Technical Publications:
Listed below are the publications associated with B22.
User Publications
These papers are all based at least in part on data gathered on beamline B22. If you have published a paper based on data from B22 which doesn't appear here, please send a reference (ideally including a DOI) to us.
23 items found for 2020 [total: 263]
Interrogation of IDH1 status in gliomas by fourier transform infrared spectroscopy Cancers, 12 Dec 2020 DOI: 10.3390/cancers12123682
Investigations of methanol-to-hydrocarbons catalysis in zeolites by synchrotron infrared microspectroscopy Dec 2020 DOI: 10.17630/sta/48
Thesis B22-Multimode InfraRed imaging And Microspectroscopy
An efficient microwave-assisted chelation (MWAC) post-synthetic modification method to produce hierarchical Y zeolites Microporous And Mesoporous Materials, 311 Oct 2020 DOI: 10.1016/j.micromeso.2020.110715
Journal Paper B22-Multimode InfraRed imaging And Microspectroscopy
Guest-controlled incommensurate modulation in a meta-rigid metal–organic framework material Journal Of The American Chemical Society, Oct 2020 DOI: 10.1021/jacs.0c08794
Post-fragmentation vesiculation timescales in hydrous rhyolitic bombs from Chaitén volcano Journal Of South American Earth Sciences, Sept 2020 DOI: 10.1016/j.jsames.2020.102807
Journal Paper B22-Multimode InfraRed imaging And Microspectroscopy
Quantitative electro-reduction of CO2 to liquid fuel over electro-synthesized metal–organic frameworks Journal Of The American Chemical Society, Sept 2020 DOI: 10.1021/jacs.0c05913
Infrared microspectroscopy and imaging analysis of inflammatory and non-inflammatory breast cancer cells and their GAG secretome Molecules, 25 Sept 2020 DOI: 10.3390/molecules25184300
Refinement of pore size at sub-angstrom precision in robust metal–organic frameworks for separation of xylenes Nature Communications, 11 Aug 2020 DOI: 10.1038/s41467-020-17640-4
Journal Paper B22-Multimode InfraRed imaging And Microspectroscopy I11-High Resolution Powder Diffraction open access
A robust metal-organic framework for gas separation Aug 2020
Thesis B22-Multimode InfraRed imaging And Microspectroscopy
Guest‐tunable dielectric sensing using a single crystal of HKUST‐1 Advanced Materials Interfaces, 7 Jul 2020 DOI: 10.1002/admi.202000408
Synthesis and characterisation of advanced porous materials for catalysis Jul 2020
Thesis B22-Multimode InfraRed imaging And Microspectroscopy I11-High Resolution Powder Diffraction
Aluminosilicate haloes preserve complex life approximately 800 million years ago Interface Focus, 10 June 2020 DOI: 10.1098/rsfs.2020.0011
Clay haloes preserve ancient fossils: An infrared view June 2020
Science Highlight B22-Multimode InfraRed imaging And Microspectroscopy
A polymer coating makes Metal Organic Frameworks better at delivering drugs June 2020
Science Highlight B22-Multimode InfraRed imaging And Microspectroscopy
Observation of binding of carbon dioxide to nitro-decorated metal–organic frameworks Chemical Science, 325 May 2020 DOI: 10.1039/C9SC04294F
Characterization of double-deformable-mirror adaptive optics for IR beam shaping in hyperspectral imaging May 2020 DOI: 10.1117/12.2554162
Synchrotron photothermal IR nanospectroscopy of macrophages drug-induced phospholipidosis Analytical Chemistry, May 2020 DOI: 10.1021/acs.analchem.9b05759
Polyamorphism mirrors polymorphism in the liquid–liquid transition of a molecular liquid Journal Of The American Chemical Society, Apr 2020 DOI: 10.1021/jacs.0c01712
Effects of crystal size on methanol to hydrocarbon conversion over single crystals of ZSM-5 studied by synchrotron infrared microspectroscopy Physical Chemistry Chemical Physics, 44 Mar 2020 DOI: 10.1039/D0CP00704H
Journal Paper B22-Multimode InfraRed imaging And Microspectroscopy
Transmission Fourier Transform Infrared (FT-IR) imaging, mapping, and synchrotron scanning microscopy with ZnS hemispheres on living mammalian cells at sub-cellular resolution Applied Spectroscopy, Feb 2020 DOI: 10.1177/0003702819898275
Journal Paper B22-Multimode InfraRed imaging And Microspectroscopy
Performances for broadband synchrotron photothermal infrared nano-spectroscopy at Diamond Light Source Infrared Physics & Technology, Feb 2020 DOI: 10.1016/j.infrared.2020.103238
Molecular identification of fungi microfossils in a Neoproterozoic shale rock Science Advances, 6 Jan 2020 DOI: 10.1126/sciadv.aax7599
Journal Paper B22-Multimode InfraRed imaging And Microspectroscopy I08-Scanning X-ray Microscopy beamline (SXM) open access
Elucidating the drug release from metal-organic framework nanocomposites via in situ synchrotron Acs Applied Materials & Interfaces, Jan 2020 DOI: 10.1021/acsami.9b21321
Journal Paper B22-Multimode InfraRed imaging And Microspectroscopy
- James M. Cameron, Justin J. A. Conn, Christopher Rinaldi, Alexandra Sala, Paul M. Brennan, Michael D. Jenkinson, Helen Caldwell, Gianfelice Cinque, Khaja Syed, Holly J. Butler, Mark G. Hegarty, David S. Palmer, Matthew J. Baker, "Interrogation of IDH1 status in gliomas by fourier transform infrared spectroscopy", Cancers, 12 (2020), DOI: 10.3390/cancers12123682
- [Thesis] Ivalina B. Minova, "Investigations of methanol-to-hydrocarbons catalysis in zeolites by synchrotron infrared microspectroscopy" (2020), DOI: 10.17630/sta/48
- Samer Abdulridha, Rongxin Zhang, Shaojun Xu, Aleksander Tedstone, Xiaoxia Ou, Jiacheng Gong, Boyang Mao, Mark Frogley, Carlo Bawn, Zhaoxia Zhou, Xinran Zhang, Sarayute Chansai, Stuart M. Holmes, Christopher Hardacre, Arthur A. Garforth, Sihai Yang, Yilai Jiao, Xiaolei Fan, "An efficient microwave-assisted chelation (MWAC) post-synthetic modification method to produce hierarchical Y zeolites", Microporous And Mesoporous Materials, 311 (2020), DOI: 10.1016/j.micromeso.2020.110715
- Jiangnan Li, Zhengyang Zhou, Xue Han, Xinran Zhang, Yong Yan, Weiyao Li, Gemma L. Smith, Yongqiang Cheng, Laura J. Mcormick Mpherson, Simon J. Teat, Mark D. Frogley, Svemir Rudic, Anibal J. Ramirez-Cuesta, Alexander J. Blake, Junliang Sun, Martin Schroeder, Sihai Yang, "Guest-controlled incommensurate modulation in a meta-rigid metal–organic framework material", Journal Of The American Chemical Society (2020), DOI: 10.1021/jacs.0c08794
- John Browning, Hugh Tuffen, Mike R. James, Jacqueline Owen, Jonathan M. Castro, Simon Halliwell, Katia Wehbe, "Post-fragmentation vesiculation timescales in hydrous rhyolitic bombs from Chaitén volcano", Journal Of South American Earth Sciences (2020), DOI: 10.1016/j.jsames.2020.102807
- Xinchen Kang, Bin Wang, Kui Hu, Kai Lyu, Xue Han, Ben F. Spencer, Mark D. Frogley, Floriana Tuna, Eric J. L. Mcinnes, Robert A. W. Dryfe, Buxing Han, Sihai Yang, Martin Schroeder, "Quantitative electro-reduction of CO2 to liquid fuel over electro-synthesized metal–organic frameworks", Journal Of The American Chemical Society (2020), DOI: 10.1021/jacs.0c05913
- Hossam Taha Mohamed, Valerie Untereiner, Gianfelice Cinque, Sherif Abdelaziz Ibrahim, Martin Götte, Nguyet Que Nguyen, Romain Rivet, Ganesh D. Sockalingum, Stephane Brezillon, "Infrared microspectroscopy and imaging analysis of inflammatory and non-inflammatory breast cancer cells and their GAG secretome", Molecules, 25 (2020), DOI: 10.3390/molecules25184300
- Xiaolin Li, Juehua Wang, Xinran Zhang, Xue Han, Ivan Da Silva, Christopher G. Morris, Shaojun Xu, Damian M. Wilary, Yinyong Sun, Yongqiang Cheng, Claire A. Murray, Chiu C. Tang, Mark D. Frogley, Gianfelice Cinque, Tristan Lowe, Haifei Zhang, Anibal J. Ramirez-Cuesta, K. Mark Thomas, Leslie W. Bolton, Sihai Yang, Martin Schroeder, Nannan Bai, "Refinement of pore size at sub-angstrom precision in robust metal–organic frameworks for separation of xylenes", Nature Communications, 11 (2020), DOI: 10.1038/s41467-020-17640-4
- [Thesis] Jiangnan Li, "A robust metal-organic framework for gas separation" (2020)
- Arun S. Babal, Abhijeet K. Chaudhari, Hamish H.-M. Yeung, Jin-Chong Tan, "Guest‐tunable dielectric sensing using a single crystal of HKUST‐1", Advanced Materials Interfaces, 7 (2020), DOI: 10.1002/admi.202000408
- [Thesis] Louis Kimberley, "Synthesis and characterisation of advanced porous materials for catalysis" (2020)
- Ross P. Anderson, Nicholas J. Tosca, Gianfelice Cinque, Mark D. Frogley, Ioannis Lekkas, Austin Akey, Gareth M. Hughes, Kristin D. Bergmann, Andrew H. Knoll, Derek E. G. Briggs, "Aluminosilicate haloes preserve complex life approximately 800 million years ago", Interface Focus, 10 (2020), DOI: 10.1098/rsfs.2020.0011
- [Science Highlight] Diamond Light Source, "Clay haloes preserve ancient fossils: An infrared view" (2020)
- [Science Highlight] Diamond Light Source, "A polymer coating makes Metal Organic Frameworks better at delivering drugs" (2020)
- Thien D. Duong, Sergey A. Sapchenko, Ivan Da Silva, Harry G. W. Godfrey, Yongqiang Cheng, Luke L. Daemen, Pascal Manuel, Mark D. Frogley, Gianfelice Cinque, Anibal J. Ramirez-Cuesta, Sihai Yang, Martin Schroeder, "Observation of binding of carbon dioxide to nitro-decorated metal–organic frameworks", Chemical Science, 325 (2020), DOI: 10.1039/C9SC04294F
- [Conference Paper] Mohammad Azizian Kalkhoran, Ann Fitzpatrick, A. Douglas Winter, Chris S. Kelley, Edmund Warrick, Mark Frogley, Gianfelice Cinque, "Characterization of double-deformable-mirror adaptive optics for IR beam shaping in hyperspectral imaging" (2020), DOI: 10.1117/12.2554162
- Ka Lung Andrew Chan, Ioannis Lekkas, Mark D. Frogley, Gianfelice Cinque, Ali Altharawi, Gianluca Bello, Lea Ann Dailey, "Synchrotron photothermal IR nanospectroscopy of macrophages drug-induced phospholipidosis", Analytical Chemistry (2020), DOI: 10.1021/acs.analchem.9b05759
- Finlay Walton, John Bolling, Andrew Farrell, Jamie Macewen, Christopher D. Syme, Mario González-Jiménez, Hans Martin Senn, Claire Wilson, Gianfelice Cinque, Klaas Wynne, "Polyamorphism mirrors polymorphism in the liquid–liquid transition of a molecular liquid", Journal Of The American Chemical Society (2020), DOI: 10.1021/jacs.0c01712
- Ivalina B. Minova, Santhosh K. Matam, Alex Greenaway, C. Richard A. Catlow, Mark D. Frogley, Gianfelice Cinque, Paul A. Wright, Russell F. Howe, "Effects of crystal size on methanol to hydrocarbon conversion over single crystals of ZSM-5 studied by synchrotron infrared microspectroscopy", Physical Chemistry Chemical Physics, 44 (2020), DOI: 10.1039/D0CP00704H
- Ka Lung Andrew Chan, Ali Altharawi, Pedro L. Fale, Cai Li Song, Sergei G. Kazarian, Gianfelice Cinque, Valerie Untereiner, Ganesh Sockalingum, "Transmission Fourier Transform Infrared (FT-IR) imaging, mapping, and synchrotron scanning microscopy with ZnS hemispheres on living mammalian cells at sub-cellular resolution", Applied Spectroscopy (2020), DOI: 10.1177/0003702819898275
- Mark D. Frogley, Ioannis Lekkas, Chris S. Kelley, Gianfelice Cinque, "Performances for broadband synchrotron photothermal infrared nano-spectroscopy at Diamond Light Source", Infrared Physics & Technology (2020), DOI: 10.1016/j.infrared.2020.103238
- S. Bonneville, F. Delpomdor, A. Préat, C. Chevalier, T. Araki, M. Kazemian, A. Steele, A. Schreiber, R. Wirth, L. G. Benning, "Molecular identification of fungi microfossils in a Neoproterozoic shale rock", Science Advances, 6 (2020), DOI: 10.1126/sciadv.aax7599
- Barbara E. Souza, Lorenzo Donà, Kirill Titov, Paolo Bruzzese, Zhixin Zeng, Yang Zhang, Arun S. Babal, Annika F. Moeslein, Mark D. Frogley, Magda Wolna, Gianfelice Cinque, Bartolomeo Civalleri, Jin-Chong Tan, "Elucidating the drug release from metal-organic framework nanocomposites via in situ synchrotron", Acs Applied Materials & Interfaces (2020), DOI: 10.1021/acsami.9b21321
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