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Structures and Surfaces
Sub-navigation
  • Structures and Surfaces
  • I05
  • B07
  • I07
  • I09

In This Section

Sub Navigation
  • Beamline Guide
    • Optical Overview
    • B07-B: NEXAFS / UHV XPS
    • B07-C: AP-XPS
      • Endstation Setup
        • Sample Holders
        • Gas Rig
        • Detectors and Analysers
        • Cells at B07-C
      • Beamline/Analyser performance
    • Sample Preparation
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Instruments by Science Group

Macromolecular
Crystallography
Soft Condensed
Matter
Imaging and
Microscopy
Biological
Cryo-Imaging
Magnetic
Materials
Structures and
Surfaces
Crystallography
Spectroscopy

B07 Contact

Principal Beamline Scientist:
Georg Held

Tel: +44 (0) 1235 778480
E-mail: [email protected]

More

Science Group Leader

Cephise Cacho

Email: [email protected]
Tel: +44 (0)1235 778290

B07 VERSOX: Versatile Soft X-ray

Status: Operational

Wavelength: 24.8 - 0.44 nm
Energy: 50 - 2800 eV

XAS: X-ray Absorption Spectroscopy XPS: X-ray Photoelectron Spectroscopy NEXAFS: Near Edge X-ray Absorption Fine Structures NAP-XPS: Near Ambient Pressure XPS Spectroscopy
  1. Instruments
  2. Structures and Surfaces
  3. B07
  4. Beamline Guide
  5. B07-C: AP-XPS
  6. Endstation Setup
  7. Detectors and Analysers

Detectors and Analysers

B07-C Ambient Pressure XPS

PHOIBOS 150 NAP Analyser

The electron energy analyser is a "PHOIBOS 150 NAP" hemispherical analyser supplied by SPECS, Berlin, Germany (left image). The analyser axis is at an angle of 60.1° with respect to the beam and tilted 30° with respect to the horizontal, i.e. close to the magic angle with respect to the polarization vector (right image). The entire assembly of interface ange and analyser is mounted on a "sledge" which can be moved parallel to the analyser axis. This way the cone-to-beam/sample distance can be changed without having to re-align the endstation, once the beam and the analyser axis have been adjusted such that they intersect in one point. The typical working distance between cone and sample is 0.2 - 0.3 mm. Compensation of residual magnetic fields is achieved via three pairs of Helmholtz coils, are individually controlled as a function of electron energy through the control unit of the electron energy analyser.

Cross secrion of PHOIBOS

Total Electron Yield – Drain current for NEXAFS

 

The entry cone of the analyser's pre-lens has an aperture of 0.3mm and is isolated from ground to allow collection of TEY NEXAFS by measuring the drain current through a Stanford Research SR 570 current amplifier (image below). In total, four currents can be recorded simultaneously:

Signal Current Amplifier (old GDA name) Current Amplifier (GDA name)
 I0 (Au mesh)  ca20 ca31c
 BLE nozzle  ca21 ca32c
 analyser cone  ca22 ca33c
 sample drain current  ca23 ca34c

 

 

test Detector layout  cone

Current Amplifier Squemes: left, centre and right

 

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