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Macromolecular
Soft Condensed 
Imaging and
Biological
Magnetic
Structures and
Crystallography 
Spectroscopy I19 Contact
Beamline Phone Number:
+44 (0) 1235 778418
Principal Beamline Scientist:
Dave Allan
Tel: +44 (0) 1235 778644
E-mail: [email protected]
Science Group Leader
Philip Chater
Email: [email protected]
Tel: +44 (0)1235 778677
I19 Small Molecule Single Crystal Diffraction
Status: Operational
Wavelength: 0.5 - 2.5 Å
Energy: 5 - 25 keV
Energy: 5 - 25 keV
User Publications
These papers are all based at least in part on data gathered on beamline I19. If you have published a paper based on data from I19 which doesn't appear here, please send a reference (ideally including a DOI) to us.
29 items found for 2010 [total: 1014]
A porphyrin fused to four anthracenes Journal Of The American Chemical Society, 133 (1) Dec 2010 DOI: 10.1021/ja109671f
Journal Paper I19-Small Molecule Single Crystal Diffraction
A dual-functional tetrakis-imidazolium macrocycle for supramolecular assembly Chemical Science, Dec 2010 DOI: 10.1039/C0SC00511H
Journal Paper I19-Small Molecule Single Crystal Diffraction
Anion recognition by highly sterically encumbered 1,2-diborylferrocenes Organometallics, 29 (21) Nov 2010 DOI: 10.1021/om1005337
Journal Paper I19-Small Molecule Single Crystal Diffraction
Self-assembly and charge transport properties of a benzobisthiazole end-capped with dihexyl thienothiophene units Journal Of Materials Chemistry, 21 (7) Nov 2010 DOI: 10.1039/C0JM02607G
Journal Paper I19-Small Molecule Single Crystal Diffraction
Investigation of the GeO2-1,6-diaminohexane-water-pyridine-HF phase diagram leading to the discovery of two novel layered germanates with extra-large rings Inorganic Chemistry, 50 (1) Nov 2010 DOI: 10.1021/ic1017505
Journal Paper I19-Small Molecule Single Crystal Diffraction
Effects of the reaction cavity on metastable optical excitation in ruthenium-sulfur dioxide complexes Physical Review B, Oct 2010 DOI: 10.1103/PhysRevB.82.155118
Journal Paper I19-Small Molecule Single Crystal Diffraction
Rotaxanes capable of recognising chloride in aqueous media Chemistry - A European Journal, Oct 2010 DOI: 10.1002/chem.201002076
Journal Paper I19-Small Molecule Single Crystal Diffraction
Multinuclear zinc pentafluorobenzene carboxylates: synthesis, characterization, and hydrogen storage capability Organometallics, 29 (22) Oct 2010 DOI: 10.1021/om100703c
Journal Paper I19-Small Molecule Single Crystal Diffraction
Yb3O(OH)6Cl.2H2O: an anion-exchangeable hydroxide with a cationic inroganic framework structure Journal Of The American Chemical Society, 132 (39) Oct 2010 DOI: 10.1021/ja104636x
Journal Paper I19-Small Molecule Single Crystal Diffraction
Structures and H2 adsorption properties of porous scandium metal-organic frameworks Chemistry - A European Journal, Oct 2010 DOI: 10.1002/chem.201000926
Journal Paper I19-Small Molecule Single Crystal Diffraction
New chiral organosulfur donors related to bis(ethylenedithio)tetrathiafulvalene Tetrahedron, 66 Sept 2010 DOI: 10.1016/j.tet.2010.06.034
Journal Paper I19-Small Molecule Single Crystal Diffraction
Synthesis and structure of pillared molybdates and tungstates with framework layers Inorganic Chemistry, 49 (18) Sept 2010 DOI: 10.1021/ic101145p
Journal Paper I19-Small Molecule Single Crystal Diffraction
A bimetallic aluminum(salen) complex for the synthesis of 1,3-oxathiolane-2-thiones and 1,3-dithiolane-2-thiones Journal Of Organic Chemistry, 75 (18) Sept 2010 DOI: 10.1021/jo101121h
Journal Paper I19-Small Molecule Single Crystal Diffraction
Surface functional polymers by post-polymerization modification using diarylcarbenes: introduction, release and regeneration of hydrogen peroxide and bactericidal activity Langmuir, 26 Sept 2010 DOI: 10.1021/la1023482
Journal Paper I19-Small Molecule Single Crystal Diffraction
Enhancement of anion recognition exhibited by a halogen-bonding rotaxane host system Journal Of The American Chemical Society, 132 (34) Aug 2010 DOI: 10.1021/ja105263q
Journal Paper I19-Small Molecule Single Crystal Diffraction
Mechanical properties of dense zeolitic imidazolate frameworks (ZIFs): a high-pressure X-ray diffraction, nanoindentation and computational study of the zinc framework Zn(Im)2, and its lithium-boron analogue, LiB(Im)4 Chemistry - A European Journal, Aug 2010 DOI: 10.1002/chem.201001415
Journal Paper I19-Small Molecule Single Crystal Diffraction
Flurbiprofen: structure and properties of (hydroxylated) Acta Crystallographica Section A Foundations of Crystallography, 66 Aug 2010 DOI: 10.1107/S010876731009817X
Conference Paper I19-Small Molecule Single Crystal Diffraction
Solid state stabilisation of the orally delivered drugs atenolol, glibenclamide, memantine and paracetamol through their complexation with cucurbit[7]uril Organic & Biomolecular Chemistry, 8 (4) Jul 2010 DOI: 10.1039/b918372h
Journal Paper I19-Small Molecule Single Crystal Diffraction
Cyclic carbonates as sustainable solvents for proline-catalysed aldol reactions Tetrahedron: Asymmetry, 21 (9-10) Jul 2010 DOI: 10.1016/j.tetasy.2010.03.051
Journal Paper I19-Small Molecule Single Crystal Diffraction
Dehydrogenation of saturated CC and BN bonds at cationic N-heterocyclic carbene stabilized M(III) centers (M = Rh, Ir) Journal Of The American Chemical Society, 132 (30) Jul 2010 DOI: 10.1021/ja1043787
Journal Paper I19-Small Molecule Single Crystal Diffraction
Expanded-ring and backbone-functionalised N-heterocyclic carbenes European Journal Of Inorganic Chemistry, 2010 (11) June 2010 DOI: 10.1002/ejic.200901182
Journal Paper I19-Small Molecule Single Crystal Diffraction
Si modified Ge-10 cluster: the preparation and characterization of single crystal Na-4(Ge,Si)(9)O-20 Crystal Research And Technology, 45 (6) May 2010 DOI: 10.1002/crat.200900746
Journal Paper I19-Small Molecule Single Crystal Diffraction
Synthesis and electropolymerization of hexadecyl functionalized bithiophene and thieno[3,2-b]thiophene end-capped with EDOT and EDTT units Chemistry Of Materials, 22 (9) May 2010 DOI: 10.1021/cm100514r
Journal Paper I19-Small Molecule Single Crystal Diffraction
Photoreactivity examined through incorporation in metal-organic frameworks Nature Chemistry, 2 (8) May 2010 DOI: 10.1038/nchem.681
Journal Paper I19-Small Molecule Single Crystal Diffraction
Bis-anthracene fused porphyrins: synthesis, crystal structure, and near-IR absorption Organic Letters, 12 (9) Apr 2010 DOI: 10.1021/ol100619p
Journal Paper I19-Small Molecule Single Crystal Diffraction
Pyridine and benzonitrile adducts of bis(4-nonafluorobiphenyl)zinc Polyhedron, 29 (1) Apr 2010 DOI: 10.1016/j.poly.2009.06.018
Journal Paper I19-Small Molecule Single Crystal Diffraction
Metal-organic polyhedral frameworks: high H2 adsorption capacities and neutron powder diffraction studies Journal Of The American Chemical Society, 132 (12) Mar 2010 DOI: 10.1021/ja1001407
Journal Paper I19-Small Molecule Single Crystal Diffraction
Heme-like coordination chemistry within nanoporous molecular crystals Science, 327 Mar 2010 DOI: 10.1126/science.1184228
Journal Paper I19-Small Molecule Single Crystal Diffraction
Benzyl N-((S)-2-hydroxy-1-{N'-[(E)-2-methoxybenzylidene]hydrazinecarbonyl}ethyl)carbamate from synchrotron data Acta Crystallographica Section E Structure Reports Online, 66 (4) Mar 2010 DOI: 10.1107/S1600536810011463
- Nicola K. S. Davis, Amber L. Thompson, Harry L. Anderson, "A porphyrin fused to four anthracenes", Journal Of The American Chemical Society, 133 (1) (2010), DOI: 10.1021/ja109671f
- Christopher J. Serpell, James Cookson, Amber L. Thompson, Paul D. Beer, "A dual-functional tetrakis-imidazolium macrocycle for supramolecular assembly", Chemical Science (2010), DOI: 10.1039/C0SC00511H
- Ian R. Morgan, Alexander E. J. Broomsgrove, Philip Fitzpatrick, Dragoslav Vidovic, Amber L. Thompson, Ian A. Fallis, Simon Aldridge, "Anion recognition by highly sterically encumbered 1,2-diborylferrocenes", Organometallics, 29 (21), 4762 - 4765 (2010), DOI: 10.1021/om1005337
- Gregg J. Mcentee, Felipe Vilela, Peter J. Skabara, Thomas D. Anthopoulos, John G. Labram, Steve Tierney, Ross W. Harrington, William Clegg, "Self-assembly and charge transport properties of a benzobisthiazole end-capped with dihexyl thienothiophene units", Journal Of Materials Chemistry, 21 (7), 2091-2097 (2010), DOI: 10.1039/C0JM02607G
- Bing Guo, Andrew Inge, Charlotte Bonneau, Junliang Sun, Kirsten Christensen, Zhong-Yong Yuan, Xiaodong Zou, "Investigation of the GeO2-1,6-diaminohexane-water-pyridine-HF phase diagram leading to the discovery of two novel layered germanates with extra-large rings", Inorganic Chemistry, 50 (1) (2010), DOI: 10.1021/ic1017505
- Anthony E. Phillips, Jacqueline M. Cole, Thierry D'Almeida, Kian Sing Low, "Effects of the reaction cavity on metastable optical excitation in ruthenium-sulfur dioxide complexes", Physical Review B (2010), DOI: 10.1103/PhysRevB.82.155118
- Laura Hancock, Lydia Gilday, Silvia Carvalho, Paulo Costa, Vitor Felix, Christopher J. Serpell, Nathan L. Kilah, Paul D. Beer, "Rotaxanes capable of recognising chloride in aqueous media", Chemistry - A European Journal (2010), DOI: 10.1002/chem.201002076
- Carl Redshaw, Surajit Jana, Congxiao Shang, Mark Elsegood, Xuesong Lu, Zheng Xiao Guo, "Multinuclear zinc pentafluorobenzene carboxylates: synthesis, characterization, and hydrogen storage capability", Organometallics, 29 (22) (2010), DOI: 10.1021/om100703c
- Helen V. Goulding, Sarah E. Hulse, William Clegg, Ross W. Harrington, Helen Y. Playford, Richard I. Walton, Andrew M. Fogg, "Yb3O(OH)6Cl.2H2O: an anion-exchangeable hydroxide with a cationic inroganic framework structure", Journal Of The American Chemical Society, 132 (39), 13618-13620 (2010), DOI: 10.1021/ja104636x
- Ilich Ibarra, Xiang Lin, Sihai Yang, Gavin S. Walker, Sarah A. Barnett, David R. Allan, Neil R. Champness, Peter Hubberstey, Martin Schroeder, Alexander J. Blake, "Structures and H2 adsorption properties of porous scandium metal-organic frameworks", Chemistry - A European Journal (2010), DOI: 10.1002/chem.201000926
- Songjie Yang, Andrew C. Brooks, Lee Martin, Peter Day, Melanie Pilkington, Ross W. Harrington, Luca Russo, John D. Wallis, William Clegg, "New chiral organosulfur donors related to bis(ethylenedithio)tetrathiafulvalene", Tetrahedron, 66, 6977-6989 (2010), DOI: 10.1016/j.tet.2010.06.034
- Jennifer L. Nicholls, Sarah E. Hulse, Samantha K. Callear, Richard A. Stephenson, William Clegg, Andrew M. Fogg, Graham J. Tizzard, Michael B. Hursthouse, Ross W. Harrington, "Synthesis and structure of pillared molybdates and tungstates with framework layers", Inorganic Chemistry, 49 (18), 8545-8551 (2010), DOI: 10.1021/ic101145p
- Ross Harrington, Michael North, Pedro Villuendas, William Clegg, "A bimetallic aluminum(salen) complex for the synthesis of 1,3-oxathiolane-2-thiones and 1,3-dithiolane-2-thiones", Journal Of Organic Chemistry, 75 (18), 6201-6207 (2010), DOI: 10.1021/jo101121h
- Jon-Paul Griffiths, Bushra Maliha, Mark G. Moloney, Amber Thompson, Ishtiaq Hussain, "Surface functional polymers by post-polymerization modification using diarylcarbenes: introduction, release and regeneration of hydrogen peroxide and bactericidal activity", Langmuir, 26, 14142 - 14153 (2010), DOI: 10.1021/la1023482
- Nathan L. Kilah, Matthew D. Wise, Christopher J. Serpell, Amber L. Thompson, Nicholas G. White, Kirsten E. Christensen, Paul D. Beer, "Enhancement of anion recognition exhibited by a halogen-bonding rotaxane host system", Journal Of The American Chemical Society, 132 (34) (2010), DOI: 10.1021/ja105263q
- Thomas D. Bennett, Jin-Chong Tan, Raimondas Galvelis, Caroline Mellot-Draznieks, Barbara Reisner, A. Thirumurugan, David. R. Allan, Anthony K. Cheetham, Stephen A. Moggach, "Mechanical properties of dense zeolitic imidazolate frameworks (ZIFs): a high-pressure X-ray diffraction, nanoindentation and computational study of the zinc framework Zn(Im)2, and its lithium-boron analogue, LiB(Im)4", Chemistry - A European Journal (2010), DOI: 10.1002/chem.201001415
- [Conference Paper] C. H. Schwalbe, M. Ramirez, B. R. Conway, C. J. Bache, S Coles, P. Timmins, "Flurbiprofen: structure and properties of (hydroxylated)", Acta Crystallographica Section A Foundations of Crystallography, 66, s85 - s85 (2010), DOI: 10.1107/S010876731009817X
- Fiona Mcinnes, Nahoum Anthony, Alan Kennedy, Nial Wheate, "Solid state stabilisation of the orally delivered drugs atenolol, glibenclamide, memantine and paracetamol through their complexation with cucurbit[7]uril", Organic & Biomolecular Chemistry, 8 (4), 765 - 773 (2010), DOI: 10.1039/b918372h
- Ross W. Harrington, Michael North, Francesca Pizzato, Pedro Villuendas, William Clegg, "Cyclic carbonates as sustainable solvents for proline-catalysed aldol reactions", Tetrahedron: Asymmetry, 21 (9-10), 1262-1271 (2010), DOI: 10.1016/j.tetasy.2010.03.051
- Christina Tang, Amber Thompson, Simon Aldridge, "Dehydrogenation of saturated CC and BN bonds at cationic N-heterocyclic carbene stabilized M(III) centers (M = Rh, Ir)", Journal Of The American Chemical Society, 132 (30) (2010), DOI: 10.1021/ja1043787
- Manuel Iglesias, Dirk J. Beetstra, Kingsley J. Cavell, Athanasia Dervisi, Ian A. Fallis, Benson M. Kariuki, Ross W. Harrington, William Clegg, Peter Horton, Simon Coles, Michael B. Hursthouse, "Expanded-ring and backbone-functionalised N-heterocyclic carbenes", European Journal Of Inorganic Chemistry, 2010 (11), 1604-1607 (2010), DOI: 10.1002/ejic.200901182
- Peng-Yan Xiao, Tie-Zhen Ren, Zhi-Qiang Wang, Kirsten Christensen, "Si modified Ge-10 cluster: the preparation and characterization of single crystal Na-4(Ge,Si)(9)O-20", Crystal Research And Technology, 45 (6), 589-592 (2010), DOI: 10.1002/crat.200900746
- Greg J. Mcentee, Peter J. Skabara, Filipe Vilela, Steven Tierney, Ifor D. W. Samuel, Salvatore Gambino, Simon Coles, Michael B. Hursthouse, Ross Harrington, William Clegg, "Synthesis and electropolymerization of hexadecyl functionalized bithiophene and thieno[3,2-b]thiophene end-capped with EDOT and EDTT units", Chemistry Of Materials, 22 (9), 3000 - 3008 (2010), DOI: 10.1021/cm100514r
- Neil Champness, Michael George, Junhua Jia, Z Cowan, Timothy Easun, Xue-Zhong Sun, Harriott Nowell, David Allan, Alexander Blake, "Photoreactivity examined through incorporation in metal-organic frameworks", Nature Chemistry, 2 (8), 688–694 (2010), DOI: 10.1038/nchem.681
- Nicola K. S. Davis, Amber L Thompson, Harry L. Anderson, "Bis-anthracene fused porphyrins: synthesis, crystal structure, and near-IR absorption", Organic Letters, 12 (9), 2124-2127 (2010), DOI: 10.1021/ol100619p
- Eddy Martin, William Clegg, Ross W. Harrington, David L. Hughes, Michael B. Hursthouse, Louise Male, Simon J. Lancaster, "Pyridine and benzonitrile adducts of bis(4-nonafluorobiphenyl)zinc", Polyhedron, 29 (1), 405 - 413 (2010), DOI: 10.1016/j.poly.2009.06.018
- Yong Yan, Irwin Telepeni, Sihai Yang, Xiang Lin, Winfried Kockelmann, Ann Dailly, William Lewis, Gavin Walker, David R. Allan, Sarah A. Barnett, Neil R. Champness, Martin Schroder, Alexander J. Blake, "Metal-organic polyhedral frameworks: high H2 adsorption capacities and neutron powder diffraction studies", Journal Of The American Chemical Society, 132 (12), 4092-4094 (2010), DOI: 10.1021/ja1001407
- C. Grazia Bezzu, Madeleine Helliwell, John E. Warren, Dave R. Allan, Neil B. Mckeown, "Heme-like coordination chemistry within nanoporous molecular crystals", Science, 327, 1627-1630 (2010), DOI: 10.1126/science.1184228
- Alessandro C. Pinheiro, Marcus V. N. De Souza, Edward R. T. Tiekind, James L. Wardell, Solange M. S. V. Wardell, "Benzyl N-((S)-2-hydroxy-1-{N'-[(E)-2-methoxybenzylidene]hydrazinecarbonyl}ethyl)carbamate from synchrotron data", Acta Crystallographica Section E Structure Reports Online, 66 (4) (2010), DOI: 10.1107/S1600536810011463
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