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Macromolecular
Soft Condensed 
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Biological
Magnetic
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Spectroscopy I15-1 Contact
Beamline Phone Number:
+44 (0) 1235 778144
Principal Beamline Scientist:
Dean Keeble
Tel: +44 (0) 1235 778391
E-mail: [email protected]
XPDF Manual
Science Group Leader
Philip Chater
Email: [email protected]
Tel: +44 (0)1235 778677
I15-1 XPDF: X-ray Pair Distribution Function
Status: Operational
Wavelength: 0.31, 0.19, 0.16 Å
Energy: 40, 65, 76 keV
Energy: 40, 65, 76 keV
These papers are all based at least in part on data gathered on beamline I15-1. If you have published a paper based on data from I15-1 which doesn't appear here, please send a reference (ideally including a DOI) to us.
32 items found for 2022 [total: 263]
Formation of a meltable purinate metal–organic framework and its glass analogue Chemical Communications, Dec 2022 DOI: 10.1039/D2CC05314D
The influence of phase purity on the stability of Pt/LaAlO3 catalysts in the aqueous phase reforming of glycerol Materials Today Chemistry, 26 Dec 2022 DOI: 10.1016/j.mtchem.2022.101230
Quantification of gas-accessible microporosity in metal-organic framework glasses Nature Communications, 13 Dec 2022 DOI: 10.1038/s41467-022-35372-5
Local structure in α-BIMEVOXes (ME = Ge, Sn) Chemistry Of Materials, 12 Dec 2022 DOI: 10.1021/acs.chemmater.2c03001
Determination of layered nickel hydroxide phases in materials disordered by stacking faults and interstratification Journal Of Materials Chemistry A, 601 Dec 2022 DOI: 10.1039/D2TA07655A
Structure dependence of fracture toughness and ionic conductivity in lithium borophosphate glassy electrolytes for all-solid-state batteries Journal Of Power Sources, 553 Nov 2022 DOI: 10.1016/j.jpowsour.2022.232302
X-ray studies of molecular structure during the crystallisation of organic salts Nov 2022
Thesis I15-1-X-ray Pair Distribution Function (XPDF)
Pair distribution function analysis of the reassembly step of the assembly-disassembly-organisation-reassembly (ADOR) process Dalton Transactions, 5 Nov 2022 DOI: 10.1039/D2DT03389E
Mapping short-range order at the nanoscale in metal–organic framework and inorganic glass composites Nanoscale, Oct 2022 DOI: 10.1039/D2NR03791B
Quinary, senary, and septenary high entropy alloy nanoparticle catalysts from core@shell nanoparticles and the significance of intraparticle heterogeneity Acs Nano, 1 Oct 2022 DOI: 10.1021/acsnano.2c07787
Journal Paper I15-1-X-ray Pair Distribution Function (XPDF)
Nanoscale insights into the structure of solution-processed graphene by X-ray scattering 2d Materials, Oct 2022 DOI: 10.1088/2053-1583/ac9b6f
Local structural distortions and reduced thermal conductivity in Ge-substituted chalcopyrite Journal Of Materials Chemistry A, 6 Oct 2022 DOI: 10.1039/D2TA06443J
Diffraction between the spots: scanning electron diffraction of beam- sensitive disordered materials Sept 2022
Thesis I15-1-X-ray Pair Distribution Function (XPDF)
The effect of framework structure and chemical functionality on melting in zeolitic imidazolate frameworks Sept 2022 DOI: 10.17863/CAM.94908
Thesis I15-1-X-ray Pair Distribution Function (XPDF)
Tetrahedral displacive disorder in the scheelite-type oxide RbReO4 Inorganic Chemistry, Sept 2022 DOI: 10.1021/acs.inorgchem.2c02282
Journal Paper I15-1-X-ray Pair Distribution Function (XPDF)
Characterisation of intergrowth in metal oxide materials using structure-mining: the case of γ-MnO 2 Dalton Transactions, 119–121 Sept 2022 DOI: 10.1039/D2DT02153F
Multicomponent, functionalized HKUST-1 analogues assembled via reticulation of prefabricated metal–organic polyhedral cavities Journal Of The American Chemical Society, Aug 2022 DOI: 10.1021/jacs.2c06131
Quick and robust PDF data acquisition using a laboratory single-crystal X-ray diffractometer for study of polynuclear lanthanide complexes in solid form and in solution Journal Of Applied Crystallography, 55 Aug 2022 DOI: 10.1107/S1600576722005878
Journal Paper I15-1-X-ray Pair Distribution Function (XPDF)
Li trapping in nanolayers of cation ‘disordered’ rock salt cathodes Journal Of Materials Chemistry A, 10 Aug 2022 DOI: 10.1039/D2TA04262B
Journal Paper I15-1-X-ray Pair Distribution Function (XPDF) I20-Scanning-X-ray spectroscopy (XAS/XES) open access
Advanced X-ray characterizations for medicine manufacturing products and processes Aug 2022
Poster I13-1-Coherence I15-1-X-ray Pair Distribution Function (XPDF)
Thermally dynamic examination of local order in nanocrystalline hydroxyapatite Journal Of Solid State Chemistry, 17 Aug 2022 DOI: 10.1016/j.jssc.2022.123474
Ambiguous structure determination from powder data: four different structural models of 4,11-difluoroquinacridone with similar X-ray powder patterns, fit to the PDF, SSNMR and DFT-D Iucrj, 9 Jul 2022 DOI: 10.1107/S2052252522004237
Quality or quantity? How structural parameters affect catalytic activity of iron oxides for CO oxidation Catalysts, 12 June 2022 DOI: 10.3390/catal12060675
Investigating pair distribution function use in analysis of nanocrystalline hydroxyapatite and carbonate-substituted hydroxyapatite Acta Crystallographica Section C Structural Chemistry, 78 May 2022 DOI: 10.1107/S2053229622003400
Revisiting vibrational spectroscopy to tackle the chemistry of Zr6O8 metal-organic framework nodes Acs Applied Materials & Interfaces, 1 May 2022 DOI: 10.1021/acsami.2c04712
The effect of Ni or Co additions on the structure of Zr60Cu30Al10 bulk metallic glass revealed by high-energy synchrotron radiation Materials Today Communications, 43 Apr 2022 DOI: 10.1016/j.mtcomm.2022.103531
Multivariate analysis of disorder in metal–organic frameworks Nature Communications, 13 Apr 2022 DOI: 10.1038/s41467-022-29849-6
Breaking with the principles of coreduction to form stoichiometric intermetallic PdCu nanoparticles Small Methods, 68 Apr 2022 DOI: 10.1002/smtd.202200420
Interfacial self-assembly of silk fibroin polypeptides and α-NiCo(OH)2 nanocrystals with tunable energy storage applications Acs Applied Electronic Materials, Mar 2022 DOI: 10.1021/acsaelm.1c01278
Journal Paper I15-1-X-ray Pair Distribution Function (XPDF)
Post-synthetic modification of a metal–organic framework glass Chemistry Of Materials, 28 Feb 2022 DOI: 10.1021/acs.chemmater.1c03820
Local structure in a tetravalent-substituent BIMEVOX system: BIGEVOX Journal Of Materials Chemistry A, 404 Jan 2022 DOI: 10.1039/D1TA07547K
Journal Paper I15-1-X-ray Pair Distribution Function (XPDF)
Principles of melting in hybrid organic-inorganic perovskite and polymorphic ABX3 structures Chemical Science, Jan 2022 DOI: 10.1039/D1SC07080K
- Alice M. Bumstead, Celia Castillo-Blas, Ignas Pakamore, Michael F. Thorne, Adam F. Sapnik, Ashleigh M. Chester, Georgina Robertson, Daniel J. M. Irving, Philip A. Chater, David A. Keen, Ross S. Forgan, Thomas D. Bennett, "Formation of a meltable purinate metal–organic framework and its glass analogue", Chemical Communications (2022), DOI: 10.1039/D2CC05314D
- D. R. Inns, X. Pei, Z. Zhou, D. J. M. Irving, S. A. Kondrat, "The influence of phase purity on the stability of Pt/LaAlO3 catalysts in the aqueous phase reforming of glycerol", Materials Today Chemistry, 26 (2022), DOI: 10.1016/j.mtchem.2022.101230
- Louis Frentzel-Beyme, Pascal Kolodzeiski, Jan-Benedikt Weiß, Andreas Schneemann, Sebastian Henke, "Quantification of gas-accessible microporosity in metal-organic framework glasses", Nature Communications, 13 (2022), DOI: 10.1038/s41467-022-35372-5
- Yajun Yue, Aleksandra Dzięgielewska, Man Zhang, Stephen Hull, Franciszek Krok, Richard M. Whiteley, Harold Toms, Marcin Malys, Xuankai Huang, Marcin Krynski, Ping Miao, Haixue Yan, Isaac Abrahams, "Local structure in α-BIMEVOXes (ME = Ge, Sn)", Chemistry Of Materials, 12 (2022), DOI: 10.1021/acs.chemmater.2c03001
- Kurt Lawson, Samuel P. Wallbridge, Amy E. Catling, Caroline A. Kirk, Sandra E. Dann, "Determination of layered nickel hydroxide phases in materials disordered by stacking faults and interstratification", Journal Of Materials Chemistry A, 601 (2022), DOI: 10.1039/D2TA07655A
- Zhimin Chen, Tao Du, Søren S. Sørensen, Rasmus Christensen, Qi Zhang, Lars R. Jensen, Oxana Magdysyuk, Maria Diaz-Lopez, Mathieu Bauchy, Yuanzheng Yue, Morten M. Smedskjaer, "Structure dependence of fracture toughness and ionic conductivity in lithium borophosphate glassy electrolytes for all-solid-state batteries", Journal Of Power Sources, 553 (2022), DOI: 10.1016/j.jpowsour.2022.232302
- [Thesis] Bethan Evans, "X-ray studies of molecular structure during the crystallisation of organic salts" (2022)
- Samantha Russell, Fanny N. Costa, Maria Diaz-Lopez, Russell E. Morris, "Pair distribution function analysis of the reassembly step of the assembly-disassembly-organisation-reassembly (ADOR) process", Dalton Transactions, 5 (2022), DOI: 10.1039/D2DT03389E
- Joonatan E. M. Laulainen, Duncan N. Johnstone, Ivan Bogachev, Louis Longley, Courtney Calahoo, Lothar Wondraczek, David A. Keen, Thomas D. Bennett, Sean M. Collins, Paul A. Midgley, "Mapping short-range order at the nanoscale in metal–organic framework and inorganic glass composites", Nanoscale (2022), DOI: 10.1039/D2NR03791B
- Sandra L. A. Bueno, Alberto Leonardi, Nabojit Kar, Kaustav Chatterjee, Xun Zhan, Changqiang Chen, Zhiyu Wang, Michael Engel, Victor Fung, Sara E. Skrabalak, "Quinary, senary, and septenary high entropy alloy nanoparticle catalysts from core@shell nanoparticles and the significance of intraparticle heterogeneity", Acs Nano, 1 (2022), DOI: 10.1021/acsnano.2c07787
- Zhengyu Yan, María Jesús García Guimarey, Khaled Parvez, Chaochao Dun, Oliver Read, Jeffrey J. Urban, Thomas Forrest, Amor Abdelkader, Cinzia Casiraghi, Wajira Mirihanage, "Nanoscale insights into the structure of solution-processed graphene by X-ray scattering", 2d Materials (2022), DOI: 10.1088/2053-1583/ac9b6f
- Sahil Tippireddy, Feridoon Azough, Vikram Vikram, Animesh Bhui, Philip Chater, Demie Kepaptsoglou, Quentin Ramasse, Robert Freer, Ricardo Grau-Crespo, Kanishka Biswas, Paz Vaqueiro, Anthony V. Powell, "Local structural distortions and reduced thermal conductivity in Ge-substituted chalcopyrite", Journal Of Materials Chemistry A, 6 (2022), DOI: 10.1039/D2TA06443J
- [Thesis] Joonatan E. M. Laulainen, "Diffraction between the spots: scanning electron diffraction of beam- sensitive disordered materials" (2022)
- [Thesis] Alice M. Bumstead, "The effect of framework structure and chemical functionality on melting in zeolitic imidazolate frameworks" (2022), DOI: 10.17863/CAM.94908
- Frederick P. Marlton, Bryce G. Mullens, Philip A. Chater, Brendan J. Kennedy, "Tetrahedral displacive disorder in the scheelite-type oxide RbReO4", Inorganic Chemistry (2022), DOI: 10.1021/acs.inorgchem.2c02282
- Nicolas P. L. Magnard, Andy Anker, Olivia Aalling-Frederiksen, Andrea Kirsch, Kirsten M. Ø. Jensen, "Characterisation of intergrowth in metal oxide materials using structure-mining: the case of γ-MnO 2", Dalton Transactions, 119–121 (2022), DOI: 10.1039/D2DT02153F
- Akim Khobotov-Bakishev, Cornelia Von Baeckmann, Borja Ortín-Rubio, Laura Hernández-López, Alba Cortés-Martínez, Jordi Martínez-Esaín, Felipe Gandara, Judith Juanhuix, Ana Platero-Prats, Jordi Faraudo, Arnau Carné-Sánchez, Daniel Maspoch, "Multicomponent, functionalized HKUST-1 analogues assembled via reticulation of prefabricated metal–organic polyhedral cavities", Journal Of The American Chemical Society (2022), DOI: 10.1021/jacs.2c06131
- Dmitry Tsymbarenko, Dimitry Grebenyuk, Maria Burlakova, Mirijam Zobel, "Quick and robust PDF data acquisition using a laboratory single-crystal X-ray diffractometer for study of polynuclear lanthanide complexes in solid form and in solution", Journal Of Applied Crystallography, 55 (2022), DOI: 10.1107/S1600576722005878
- Maria Diaz-Lopez, Philip A. Chater, Olivier Proux, Yves Joly, Jean-Louis Hazemann, Pierre Bordet, Valerie Pralong, "Li trapping in nanolayers of cation ‘disordered’ rock salt cathodes", Journal Of Materials Chemistry A, 10, 17415 - 17423 (2022), DOI: 10.1039/D2TA04262B
- [Poster] D. Saha, "Advanced X-ray characterizations for medicine manufacturing products and processes" (2022)
- Emily L. Arnold, Sarah Gosling, Samantha K. Davies, Hannah L. Cross, Paul Evans, Dean S. Keeble, Charlene Greenwood, Keith D. Rogers, "Thermally dynamic examination of local order in nanocrystalline hydroxyapatite", Journal Of Solid State Chemistry, 17 (2022), DOI: 10.1016/j.jssc.2022.123474
- Carina Schlesinger, Arnd Fitterer, Christian Buchsbaum, Stefan Habermehl, Michele R. Chierotti, Carlo Nervi, Martin U. Schmidt, "Ambiguous structure determination from powder data: four different structural models of 4,11-difluoroquinacridone with similar X-ray powder patterns, fit to the PDF, SSNMR and DFT-D", Iucrj, 9 (2022), DOI: 10.1107/S2052252522004237
- Steffen Schlicher, Nils Prinz, Julius Bürger, Andreas Omlor, Christian Singer, Mirijam Zobel, Roland Schoch, Jörg K. N. Lindner, Volker Schünemann, Sven Kureti, Matthias Bauer, "Quality or quantity? How structural parameters affect catalytic activity of iron oxides for CO oxidation", Catalysts, 12 (2022), DOI: 10.3390/catal12060675
- Emily L. Arnold, Dean S. Keeble, J. P. O. Evans, Charlene Greenwood, Keith D. Rogers, "Investigating pair distribution function use in analysis of nanocrystalline hydroxyapatite and carbonate-substituted hydroxyapatite", Acta Crystallographica Section C Structural Chemistry, 78 (2022), DOI: 10.1107/S2053229622003400
- Ignacio Romero-Muniz, Carlos Romero-Muñiz, Isabel Del Castillo-Velilla, Carlo Marini, Sofía Calero, Félix Zamora, Ana Platero-Prats, "Revisiting vibrational spectroscopy to tackle the chemistry of Zr6O8 metal-organic framework nodes", Acs Applied Materials & Interfaces, 1 (2022), DOI: 10.1021/acsami.2c04712
- Martin E. Stiehler, Nikolaos T. Panagiotopoulos, Dean S. Keeble, Yurii P. Ivanov, Melita Menelaou, Mark R. Jolly, A. Lindsay Greer, Konstantinos Georgarakis, "The effect of Ni or Co additions on the structure of Zr60Cu30Al10 bulk metallic glass revealed by high-energy synchrotron radiation", Materials Today Communications, 43 (2022), DOI: 10.1016/j.mtcomm.2022.103531
- Adam F. Sapnik, Irene Bechis, Alice M. Bumstead, Timothy Johnson, Philip A. Chater, David A. Keen, Kim E. Jelfs, Thomas Bennett, "Multivariate analysis of disorder in metal–organic frameworks", Nature Communications, 13 (2022), DOI: 10.1038/s41467-022-29849-6
- Jette K. Mathiesen, Espen D. Bøjesen, Jack K. Pedersen, Emil T. S. Kjær, Mikkel Juelsholt, Susan Cooper, Jonathan Quinson, Andy S. Anker, Geoff Cutts, Dean S. Keeble, Maria S. Thomsen, Jan Rossmeisl, Kirsten M. Ø. Jensen, "Breaking with the principles of coreduction to form stoichiometric intermetallic PdCu nanoparticles", Small Methods, 68 (2022), DOI: 10.1002/smtd.202200420
- Eduardo R. Do Nascimento, Barbara B. Gerbelli, Fabio F. Ferreira, Fanny N. Costa, Philip A. Chater, Wendel A. Alves, "Interfacial self-assembly of silk fibroin polypeptides and α-NiCo(OH)2 nanocrystals with tunable energy storage applications", Acs Applied Electronic Materials (2022), DOI: 10.1021/acsaelm.1c01278
- Alice M. Bumstead, Ignas Pakamore, Kieran D. Richards, Michael F. Thorne, Sophia S. Boyadjieva, Celia Castillo-Blas, Lauren N. Mchugh, Adam F. Sapnik, Dean S. Keeble, David A. Keen, Rachel C. Evans, Ross S. Forgan, Thomas D. Bennett, "Post-synthetic modification of a metal–organic framework glass", Chemistry Of Materials, 28 (2022), DOI: 10.1021/acs.chemmater.1c03820
- Yajun Yue, Aleksandra Dzięgielewska, Stephen Hull, Franciszek Krok, Richard M. Whiteley, Harold Toms, Marcin Malys, Man Zhang, Haixue Yan, Isaac Abrahams, "Local structure in a tetravalent-substituent BIMEVOX system: BIGEVOX", Journal Of Materials Chemistry A, 404 (2022), DOI: 10.1039/D1TA07547K
- Bikash Kumar Shaw, Thomas D. Bennett, Celia Castillo-Blas, Michael F. Thorne, María Laura Ríos Gómez, Thomas Forrest, David A. Keen, Maria Diaz-Lopez, Philip A. Chater, Lauren N. Mchugh, "Principles of melting in hybrid organic-inorganic perovskite and polymorphic ABX3 structures", Chemical Science (2022), DOI: 10.1039/D1SC07080K
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