Beamlines | I22 - Facility and Equipment availability

End Station

Last updated: 1 September 2010

Equipment or Component
Availability
Comments
Camera length 5 m
Available
Can access wide q range by changing energy
Camera length 1.2 m
Available
May require additional commissioning time for focusing.
Camera length 9 m
Commissioning (2010)
Intermediate camera lengths to follow, will require additional commissioning time for focusing.
Energy range 7-15 keV
Available
 
Energy range 3.7 – 7 keV
Available
 
No vacuum sample environment available unless user supplied for experiments below 5keV*
Energy range 15 – 20 keV
Available
 
Large sample table (100 kg)
Available
Travel of table is ± 100 mm in vertical and horizontal directions
Precision XY translation stage (2 kg)
Available
Travel of table is ± 50 mm in vertical and horizontal directions
Rotation stage
Available
0° to 360°
Detectors
RAPID
Available
2D SAXS detector
HOTSAXS
Available
1D SAXS detector
HOTWAXS
Available
1D WAXS detector
MARCCD
Available
2D SAXS detector
Fast shutter
Commissioning
 
Microfocus end station
Available
 
Inline microscope
In design
 
Keyence Sample Vision System
Commissioning
 

* Restrictions apply. Please contact beamline staff well in advance to discuss feasibility.

Sample Environments

18 position sample changer
Available
 
Heated sample changer (10-150°C)
Commissioning
 
Capillary sample changer
Available
 
Liquid cell holder
Available
 
Solid sample grid (large holes)
Available
 
Solid sample grid (small holes)
Available
 
Water bath
Available
 
DSC
Available
 
Linkam capillary stage
Available
 
Stopped Flow – 4 syringe
Available
Stand alone control by proprietary software
Rheometer
Available
Stand alone control by proprietary software
Cryojet
Available
 
Furnace
Commissioning
 
Available
 
HPLC
Commissioning
 

Support Facilities

Chemistry lab including fume hood
Available
Standard lab solvents and reagents, synthesis glassware and sample preparation equipment available
Fridge and freezer (-20°C)
Available
 
Glovebox - wet, oxygen free
Available
 
Ultrapure water (18.2MW )
Available
 
Balances (4 d.p.)
Available
 
Binocular Microscope
Available
 
Nanodrop UV-vis spectrophotometer
Available
 
Tensiometer
Available
 
Vacuum oven
Available
 
Rotary evaporator
Available
 
Centrifuge
Available
 
Drying oven
Available
 
pH meters
Available
 
Water bath, heating mantles, stirrers, ultrasound bath
Available
 

For any further information, please contact a member of the beamline staff.