Beamlines | I19 - Facility and Equipment Availability

Experimental Hutch 1

Last updated: 18 October 2011

Equipment or Component Availability
Comments
4-circle diffractometer & CCD detector
Available
Currently optimising.
Robotic sample changer
Available
Automated sample changing is now available for samples that are stable in air at ambient temperature. Optimisation is ongoing to allow fully automated data collection.
Energy range 10-22 keV
Available
18 keV is the standard set up, it is likely that energies down to ~ 7 keV will be available early in 2011.
Energy range 5 - 10 keV and 22 - 25 keV
2012 Available with focussing from 2012.
Rigaku Saturn
Available
CCD for EH1 diffractometer
Stereomicroscope
Available
 

* Restrictions apply. Please contact beamline staff well in advance.

Experimental Hutch 2

Equipment or Component Availability
Comments
4-circle diffractometer & CCD detector
Available
Currently optimising.
Energy range 10 - 22 keV
Available
18 keV is the standard set-up
Energy range 5 - 10 keV and 22 - 25 keV
2012 Available with focussing from 2012.
Oxford Atlas CCD
Available
CCD for EH2 diffractometer
Pilatus 300K detector
Commissioning 2011 - 2012
Photon counting detector available from October 2012.

* Restrictions apply. Please contact beamline staff well in advance.

Sample Environments

Cryostream for EH1
Available 
 
Helix for EH1 Available  
Cryostream for EH2 Available  
Helix for EH2 Commissioning
 
Hot air blower for EH2 Commissioning 2012  
Cryostat for EH2 diffractometer Optimising 2011  
Open flow helium device in EH2 Commissioning 2011 Available from 2012
Gas Cell Available  
Diamond anvil cell Available  

Support Facilities

Chemistry lab including fume hood
Available
 
Fridge (5 °C) and freezer (-20 °C)
Available
 
Glovebox - H2O, O2 free
Available
 
Ultrapure water (18.2MW )
Available
 
Balance (5 d.p.)
Available
 
Stereomicroscopes
Available
 
Drying oven (up to 300 °C)
Available
 
Hotplate Stirrers
Available
 
Melting Point
Available
 
Ruby Fluorescence spectrometer Available  
Gasket hole driller for Diamond anvil cell preparation Available  
Schlenk line Available  
X-Temp 2 crystal cooling device Available  
N2 blower Available  

Restrictions apply. Please contact a member of the beamline staff well in advance to discuss feasibility.