Beamlines | I15 - Facility and Equipment availability

Experimental Hutch - View panorama

Equipment or Component

Availability

Comments

EH: 6-circle Newport diffractometer with dummy cell

close-up upstream view (DAC)

close-up downstream view (DAC)

single crystal in air: upstream and downstream view

Restricted motions due to mounts.

Omega and phi scans for single crystal diffraction available.

Important: sample co-ordinate system is NOT identical to x-ray beam co-ordinate system.

EH: Second Table (micro-focussing option)

 

Available soon Sample motions and micro-focussing available soon.

Perkin Elmer flat panel 1621 EN detector

2048 x 2048 pixels (0.2mm pixel size)

Available

Weak and overexposed reflections might cause problems. Images can be recorded while DAC is rocking. Software used for integration of images is Fit2D. A tutorial video how to calibrate wavelenght and detector-to-sample distance can be found here. This video uses input parameters for the PE detector.

Atlas CCD Oxford diffraction. Mainly used for single-crystal x-ray but available for powder diffraction on demand.

For experienced single-crystal users. Knowledge of Crysalis software advantageous.

Software and hardware for single-crystal collection is under development. Software used for analysis is Crysalis. Note: Crystals may suffer radiation damage.

MAR 345 image plate

3450 x 3450 'pixels' (0.1mm 'pixel' size in standard configuration)

Available

Images can be recorded while DAC is rocking. Software used for integration of image is Fit2D. A tutorial video how to calibrate wavelenght and detector-to-sample distance can be found here. This video uses input parameters for the PE detector.

"standard" V-block mount for Diamond-Anvil Cells (side- and top-view)

Users requested to provide their own (DAC)

 

Requires a 50 mm or 60 mm diameter DAC to fit a specific V-block for the diffractometer. A standard Huber goniometer head (model numbers 1003 and 1004) can be mounted. Any other mount needs to be specified well in advance of experiment.

On-line pressure measurement via optical fibres. Available 473 nm laser.

Pressure measurement off-line, Horiba Jobin-Yvon (iHR320) spectrometer and fibre coupled laser.

Available

473 nm laser, sensitive for ruby fluorescence to 100 GPa.

A sample preparation area is equipped with basic tools to load cells.

Available

Microscope available, fluid/solid media sample management, and gasket preparation (spark erosion and mechanical drilling).

Glove box (microscope attached) Available Inert gas

Peripheral labs

Available

Off-line Raman

White-beam Available on request  

For any further information, please contact a member of the beamline staff.