Beamlines | I15 - Facility and Equipment availability

Restrictions apply. Users requested to bring own DAC.

Please contact beamline staff well in advance to discuss feasibility.

Experimental Hutch - View panorama

Equipment or Component

Availability

Comments

EH1: 6-circle Newport diffractometer

Available but motion restricted by mounts.

Important: sample co-ordinate system is NOT identical to x-ray beam co-ordinate system.

MAR 345 image plate mounted on diffractometer. Effective ‘pixel size’ of 0.1mm

Available

Images can be recorded while DAC is rocking typ, +/- 3 degrees. Software used for integration of image is Fit2D.

Ruby CCD Oxford diffraction Pixel size at scintillator 48μm. Used for single-crystal x-ray and rapid powder diffraction. Mounted on the diffractometer on demand (interchangeable with image plate only).

CCD - Limited phi scans, but No single-crystal experiments needing full-refinement of intensity data

  • Powder on demand
  • Single crystals with limited rotation scans

Software and hardware for single-crystal collection is under development.

Software used for analysis is Crysalis.

EH2: Second-Station Table and Micro-focus beam delivery

Not available before end 2010

 

White-beam station

No permanent station or detector provision available before 2011.

Contact I15 staff.

Users requested to provide own Diamond-Anvil Cell (DAC)

N/A

Requires a 50 mm or 60 mm diameter DAC to fit a specific V-block for the diffractometer. A standard Huber goniometer head (model numbers 1003 and 1004) can be mounted. Any other mount needs to be specified well in advance of experiment.

Pressure measurement using off-line ruby fluorescence method based on a HR320 (Horiba Jobin-Yvon) spectrometer and fibre coupled lasers (532nm and 487nm)

Available

 

Sensitive for ruby fluorescence to 100 GPa

A sample preparation area adjacent to Beamline workstation in control cabin CC2 is equipped with basic tools to load cells.

Available

Microscope available and fluid/solid media sample management and gasket preparation.

On-line pressure measurement via optical fibres

Available


Peripheral labs

2010

Off-line Raman and Laser Heating

For any further information, please contact a member of the beamline staff.