I14 sample holders are designed to take standard silicon nitride membranes in the following sizes
5 x 5 mm Frame with 3 mm window
7.5 x 7.5mm Frame with 3 mm window
Typical window thickness ranges from 200nm - 1um with the thicker windows being slightly more robust.
The beamline can supply standard membranes for testing on request.
A variety of silicon nitride membranes options are available from commercial suppliers with designs and options to suit different applications.
Please contact the beamline team to discuss any specific requirements before your experiment and sample preparation.
Silicon Nitride Membrane suppliers
I14 sample holders are designed to take 3mm TEM grids.
Both full and half (e.g. omniprobe) grids can be mounted.
The thickness of the grids varies and ring spacers are available at the beamline to aid mounting if required.
For XRF mapping consideration should be given to the grid material. While copper is the most common grid material, Nickel and Gold are also avaiable which may be more beneficial depending on how your sample is mounted on the grid and the elements of interest to you.
TEM grid suppliers:
Diamond Light Source is the UK's national synchrotron science facility, located at the Harwell Science and Innovation Campus in Oxfordshire.
Copyright © 2017 Diamond Light Source
Diamond Light Source Ltd
Harwell Science & Innovation Campus