Oxana Magdysyuk

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Oxana Magdysyuk is a Support Scientist on I12.

Email: oxana.magdysyuk@diamond.ac.uk
Tel: +44 (0) 1235 778717

Key Research Area

Key Research Interests

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  1. Research Expertise
  2. Collaborations
  3. Selected publications:
Research Expertise -

Research Expertise

 

in situ investigation of gas adsorption in porous materials by powder diffraction.

– structure solution from powder diffraction data.

in situ investigation of structural phase transitions by powder diffraction: parametric Rietveld refinement and strain/order parameter coupling.

– electron density distribution by maximum entropy method.

– incommensurate modulated structures from single crystal diffraction.

Collaborations - +

Collaborations

Selected publications: - +

 

1) Oh, H.; Maurer, S.; Balderas-Xicohtencatl, R.; Arnold, L.; Magdysyuk, O. V.; Schuetz, G.; Mueller, U.; Hirscher, M. Efficient synthesis for large-scale production and characterization for hydrogen storage of ligand exchanged MOF-74/174/184-M (M = Mg2+, Ni2+). International Journal of Hydrogen energy. 2017, 42(2), 1027–1035.

2) Dud, M.; Magdysyuk, O.V.; Margetic, D.; Strukil, V. Synthesis of monosubstituted thioureas by vapour digestion and mechanochemical amination of thiocarbamoyl benzotriazoles. Green Chem. 2016, 18, 2666–2674.

3) Schmieder, P.; Denysenko, D.; Grzywa, M.; Magdysyuk, O.; Volkmer, D. A structurally flexible triazolate-based metal–organic framework featuring coordinatively unsaturated copper(I) sites. Dalton Trans. 2016, 45, 13853–13862.

4) Pogosova, M.A.; Kalachev, I.L.; Eliseev, A.A.; Magdysyuk, O.V.; Dinnebier, R.E.; Jansen, M.; Kazin, P.E. Synthesis and characterization of the copper doped Ca-La apatites. Dyes and Pigments. 2016, 133, 109–113.

5) Kazin, P.E.; Pogosova, M.A.; Trusov, L.A.; Kolesnik, I.V.; Magdysyuk, O.V.; Dinnebier, R.E. Crystal structure details of La- and Bi-substituted hydroxyapatites: Evidence for LaO+ and BiO+ with a very short metal–oxygen bond. Journal of Solid State Chemistry. 2016, 237, 349–357.

6) Strukil, V.; Gracin, D.; Magdysyuk, O.V.; Dinnebier, R.E.; Friscic, T. Trapping Reactive Intermediates by Mechanochemistry: Elusive Aryl N‐Thiocarbamoylbenzotriazoles as Bench‐Stable Reagents. Angew.Chem., Int.Ed., 2015, 54, 8440–8443.

7) Drakopoulos, M.; Connolley, Th.; Reinhard, C.; Atwood, R.; Magdysyuk, O.; Vo, N.; Hart, M.; Connor, L.; Humphreys, B.; Howell, G.; Davies, S.; Hill, T.; Wilkin, G.; Pedersen, U.; Foster, A.; De Maio, N.; Basham, M.; Yuan, F.; Wanelik, K. I12: the Joint Engineering, Environment and Processing (JEEP) beamline at Diamond Light Source. J. Synchrotron Rad. 2015, 22(3), 828-838.

8) Magdysyuk, O.V.; Denysenko, D.; Weinrauch, I.; Volkmer, D.; Hirscher, D.; Dinnebier, R.E. Formation of a quasi-solid structure by intercalated noble gas atoms in pores of CuI-MFU-4l metal-organic framework. Chem. Commun. 2014, 51, 714–717.

9) Magdysyuk, O.V.; Adams, F.; Liermann, H-P.; Spanopoulos, I.; Trikalitis, P.N.; Hirscher, D.; Morris, R.E.; Duncan, M.J.; McCormic, L.J.; Dinnebier, R.E. Understanding the adsorption mechanism of noble gases Kr and Xe in CPO-27-Ni, CPO-27-Mg, and ZIF-8. Phys.Chem.Chem.Phys. 2014, 16, 23908–23914.

10) Magdysyuk, O.V.; Mueller, M.; Dinnebier; R.E.; Lipp, C.; Schleid, Th. Parameterization of the coupling between strain and order parameter for LuF[SeO3]. J. Appl. Cryst. 2014, 47, 701–711.

11) Greiner, S.; Chou, S.; Magdysyuk, O.V.; Dinnebier, R.E.; Schleid, Th. Structural phase transitions in ScF[SeO3] and YF[SeO3]. Z. Anorg. Allgem. Chemie. 2014, 640, 3203–3211.

12) Kazin, P.E.; Zykin, M.A.; Zubavichus, Y.V.; Magdysyuk, O.V.; Dinnebier; R.E.; Jansen, M. Identification of the Chromophore in the Apatite Pigment [Sr10(PO4)6(CuxOH1-x-y)2]: Linear OCuO Featuring a Resonance Raman Effect, an Extreme Magnetic Anisotropy, and Slow Spin Relaxation. Chem. Eur. J. 2014, 20, 165–178.

13) Magdysyuk, O.V.; Nuss, J.; Jansen, M. Modulated crystal structure of Pr2SbO2. Acta Cryst. 2013, B69, 547–555.

14) Soleimani-Dorcheh, A.; Dinnebier, R.E.; Kuc, A.; Magdysyuk, O.V.; Adams, F.; Denysenko, D.; Heine, Th.; Volkmer, D.; Donner, W.; Hirscher, M. Novel characterization of the adsorption sites in large pore metal-organic frameworks: combination of X-ray powder diffraction and thermal desorption spectroscopy. Phys.Chem.Chem.Phys., 2012, 14(37), 12892–12897.

15) Magdysyuk, O.V.; Dinnebier; R.E.; van Smaalen, S.; Zykin, M.A.; Kazin, P.E.; Jansen, M. Reconstructions of electron density by the Maximum Entropy Method from X-ray powder diffraction data based on incomplete and complete crystal structure models: a case study of apatites with different intercalated metal atoms. Z. Kristallog. 2012, 227, 321–333.

16) Runcevski, T.; Dinnebier; R.E.; Magdysyuk, O.V.; Pollmann, H. Crystal structures of calcium hemicarboaluminate and carbonated calcium hemicarboaluminate from synchrotron powder diffraction data. Acta Cryst. 2012, B68, 493–500.

17) Kazin, P.E.; Zykin, M.A.; Dinnebier; R.E.; Magdysyuk, O.V.; Tretyakov Y.D.; Jansen, M. An Unprecedented Process of Peroxide Ion Formation and its Localization in the Crystal Structure of Strontium Peroxy-Hydroxyapatite Sr10(PO4)6(O2)x(OH)2-2x. Z. anorg. allgem. chemie. 2012, 638(6), 909–919.